(S,5Z)-tert-butyl 4-((R)-1-amino-6-((tert-butoxycarbonyl)amino)-10,10-dimethyl-1,8-dioxo-2,9-dioxa-5,7-diazaundec-6-en-4-yl)-3-benzyl-5-(3-(benzyloxy)propylidene)-2-((tert-butoxycarbonyl)imino)imidazolidine-1-carboxylate

Base Information

Chemical Name:(S,5Z)-tert-butyl 4-((R)-1-amino-6-((tert-butoxycarbonyl)amino)-10,10-dimethyl-1,8-dioxo-2,9-dioxa-5,7-diazaundec-6-en-4-yl)-3-benzyl-5-(3-(benzyloxy)propylidene)-2-((tert-butoxycarbonyl)imino)imidazolidine-1-carboxylate
CAS No.:1350560-15-4
Molecular Formula:C₄₄H₆₃N₇O₁₁
Molecular Weight:866.025
Hs Code.:

(S,5Z)-tert-butyl 4-((R)-1-amino-6-((tert-butoxycarbonyl)amino)-10,10-dimethyl-1,8-dioxo-2,9-dioxa-5,7-diazaundec-6-en-4-yl)-3-benzyl-5-(3-(benzyloxy)propylidene)-2-((tert-butoxycarbonyl)imino)imidazolidine-1-carboxylate

Synonyms:(S,5Z)-tert-butyl 4-((R)-1-amino-6-((tert-butoxycarbonyl)amino)-10,10-dimethyl-1,8-dioxo-2,9-dioxa-5,7-diazaundec-6-en-4-yl)-3-benzyl-5-(3-(benzyloxy)propylidene)-2-((tert-butoxycarbonyl)imino)imidazolidine-1-carboxylate

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Chemical Property of (S,5Z)-tert-butyl 4-((R)-1-amino-6-((tert-butoxycarbonyl)amino)-10,10-dimethyl-1,8-dioxo-2,9-dioxa-5,7-diazaundec-6-en-4-yl)-3-benzyl-5-(3-(benzyloxy)propylidene)-2-((tert-butoxycarbonyl)imino)imidazolidine-1-carboxylate

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Technology Process of (S,5Z)-tert-butyl 4-((R)-1-amino-6-((tert-butoxycarbonyl)amino)-10,10-dimethyl-1,8-dioxo-2,9-dioxa-5,7-diazaundec-6-en-4-yl)-3-benzyl-5-(3-(benzyloxy)propylidene)-2-((tert-butoxycarbonyl)imino)imidazolidine-1-carboxylate

There total 7 articles about (S,5Z)-tert-butyl 4-((R)-1-amino-6-((tert-butoxycarbonyl)amino)-10,10-dimethyl-1,8-dioxo-2,9-dioxa-5,7-diazaundec-6-en-4-yl)-3-benzyl-5-(3-(benzyloxy)propylidene)-2-((tert-butoxycarbonyl)imino)imidazolidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1350560-14-3
C₄₄H₆₃N₇O₁₁

: 1350560-15-4
(S,5Z)-tert-butyl 4-((R)-1-amino-6-((tert-butoxycarbonyl)amino)-10,10-dimethyl-1,8-dioxo-2,9-dioxa-5,7-diazaundec-6-en-4-yl)-3-benzyl-5-(3-(benzyloxy)propylidene)-2-((tert-butoxycarbonyl)imino)imidazolidine-1-carboxylate

Guidance literature:: With silver(I) acetate; In dichloromethane; at 20 ℃;
DOI:10.1021/ja2098063

Reference yield:

: (2R,3R)-2-amino-3-(benzylamino)-7-(benzyloxy)hept-4-yn-1-ol bis-hydrochloride

: 1350560-15-4
(S,5Z)-tert-butyl 4-((R)-1-amino-6-((tert-butoxycarbonyl)amino)-10,10-dimethyl-1,8-dioxo-2,9-dioxa-5,7-diazaundec-6-en-4-yl)-3-benzyl-5-(3-(benzyloxy)propylidene)-2-((tert-butoxycarbonyl)imino)imidazolidine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanesulfonic acid / dichloromethane / 2.17 h / 0 °C

1.2: pH Ca_. 10 / Cooling with ice

2.1: triethylamine; mercury(II) oxide / dichloromethane / 8 h / 20 °C

3.1: silver(I) acetate / dichloromethane / 20 °C

With methanesulfonic acid; silver(I) acetate; triethylamine; mercury(II) oxide; In dichloromethane;
DOI:10.1021/ja2098063

Reference yield:

: 1350560-23-4
tert-butyl ((2R,3R)-3-(benzylamino)-7-(benzyloxy)-1((tert-butyldiphenylsilyl)oxy)hept-4-yn-2-yl)carbamate

: 1350560-15-4
(S,5Z)-tert-butyl 4-((R)-1-amino-6-((tert-butoxycarbonyl)amino)-10,10-dimethyl-1,8-dioxo-2,9-dioxa-5,7-diazaundec-6-en-4-yl)-3-benzyl-5-(3-(benzyloxy)propylidene)-2-((tert-butoxycarbonyl)imino)imidazolidine-1-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / methanol / 12 h / 40 °C

2.1: methanesulfonic acid / dichloromethane / 2.17 h / 0 °C

2.2: pH Ca_. 10 / Cooling with ice

3.1: triethylamine; mercury(II) oxide / dichloromethane / 8 h / 20 °C

4.1: silver(I) acetate / dichloromethane / 20 °C

With hydrogenchloride; methanesulfonic acid; silver(I) acetate; triethylamine; mercury(II) oxide; In methanol; dichloromethane;
DOI:10.1021/ja2098063