bis(2,3-dimethyl-1,4-bis(2,6-diisopropylphenyl)-1,4-diaza-1,3-butadiene^(1-))iron(II)

Base Information

• Chemical Name: bis(2,3-dimethyl-1,4-bis(2,6-diisopropylphenyl)-1,4-diaza-1,3-butadiene^(1-))iron(II)
• CAS No.: 869986-09-4
• Molecular Formula: C₅₆H₈₀FeN₄
• Molecular Weight: 865.125

Synonyms:bis(2,3-dimethyl-1,4-bis(2,6-diisopropylphenyl)-1,4-diaza-1,3-butadiene^(1-))iron(II)

Chemical Property of bis(2,3-dimethyl-1,4-bis(2,6-diisopropylphenyl)-1,4-diaza-1,3-butadiene^(1-))iron(II)

Chemical Property:

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MSDS Files:

SDS file from LookChem

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Technology Process of bis(2,3-dimethyl-1,4-bis(2,6-diisopropylphenyl)-1,4-diaza-1,3-butadiene^(1-))iron(II)

There total 1 articles about bis(2,3-dimethyl-1,4-bis(2,6-diisopropylphenyl)-1,4-diaza-1,3-butadiene^(1-))iron(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1,4-di(2,6-diisopropylphenyl)-2,3-dimethyl-1,4-diazabutadiene + dichloro(2,3-dimethyl-1,4-bis(2,6-diisopropylphenyl)-1,4-diaza-1,3-butadiene)iron(II) (99442-41-8) → bis(2,3-dimethyl-1,4-bis(2,6-diisopropylphenyl)-1,4-diaza-1,3-butadiene(1-))iron(II) (869986-09-4)

Guidance literature:

With Na; Hg; In pentane; byproducts: NaCl, Fe; (N2); Schlenk technique; Na was added with stirring to Hg in pentane; stirred for 10 min; Fe complex was added; stirred for 24 h; ligand was added; mixt. was stirred for 24 h; decanted; filtered through Celite; volatiles removed (vac.); recrystd. (pentane); elem. anal.;

DOI:10.1021/om050625b

Reference yield:

bis(2,3-dimethyl-1,4-bis(2,6-diisopropylphenyl)-1,4-diaza-1,3-butadiene(1-))iron(II) (869986-09-4) + carbon monoxide (201230-82-2) → diiron nonacarbonyl (15321-51-4) + iron pentacarbonyl (13463-40-6,71564-23-3,37220-42-1) + [2,6-(CHMe2)2-C6H3N=C(Me)C(Me)=N-2,6-(CHMe2)2-C6H3]Fe(CO)3 (658063-27-5)

Guidance literature:

In not given; byproducts: 2,6-(CHMe2)2-C6H3N=C(Me)C(Me)=N-2,6-(CHMe2)2-C6H3; Fe complex was treated with CO (1 atm);

DOI:10.1021/om050625b

upstream raw materials:

dichloro(2,3-dimethyl-1,4-bis(2,6-diisopropylphenyl)-1,4-diaza-1,3-butadiene)iron(II)

Downstream raw materials:

diiron nonacarbonyl

iron pentacarbonyl

[2,6-(CHMe₂)2-C₆H₃N=C(Me)C(Me)=N-2,6-(CHMe₂)2-C₆H₃]Fe(CO)3

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