trimethyl 3,3',3''-[1,3,5-benzenetriyltris(methylenesulfinyl)]trispropanoate

Base Information

Chemical Name:trimethyl 3,3',3''-[1,3,5-benzenetriyltris(methylenesulfinyl)]trispropanoate
CAS No.:1297502-17-0
Molecular Formula:C₂₁H₃₀O₉S₃
Molecular Weight:522.662
Hs Code.:

Synonyms:trimethyl 3,3',3''-[1,3,5-benzenetriyltris(methylenesulfinyl)]trispropanoate

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Chemical Property of trimethyl 3,3',3''-[1,3,5-benzenetriyltris(methylenesulfinyl)]trispropanoate

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Technology Process of trimethyl 3,3',3''-[1,3,5-benzenetriyltris(methylenesulfinyl)]trispropanoate

There total 2 articles about trimethyl 3,3',3''-[1,3,5-benzenetriyltris(methylenesulfinyl)]trispropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1,3,5-tri-{[(2-methoxycarbonylethyl)thio]methyl}benzene

: 1297502-17-0
trimethyl 3,3',3''-[1,3,5-benzenetriyltris(methylenesulfinyl)]trispropanoate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 ℃;
DOI:10.1016/j.bmc.2012.03.070

Reference yield:

: 38460-57-0
1,3,5-tris(mercaptomethyl)benzene

: 1297502-17-0
trimethyl 3,3',3''-[1,3,5-benzenetriyltris(methylenesulfinyl)]trispropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: N-benzyl-trimethylammonium hydroxide / tetrahydrofuran; methanol / 0.5 h / -78 °C / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -78 °C

With N-benzyl-trimethylammonium hydroxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1055/s-0030-1259306