4-{[1-(3-bromo-phenyl)-meth-(E)-ylidene]-amino}-benzoic acid methyl ester

Base Information

Chemical Name:4-{[1-(3-bromo-phenyl)-meth-(E)-ylidene]-amino}-benzoic acid methyl ester
CAS No.:1391608-87-9
Molecular Formula:C₁₅H₁₂BrNO₂
Molecular Weight:318.17
Hs Code.:

Synonyms:4-{[1-(3-bromo-phenyl)-meth-(E)-ylidene]-amino}-benzoic acid methyl ester

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Chemical Property of 4-{[1-(3-bromo-phenyl)-meth-(E)-ylidene]-amino}-benzoic acid methyl ester

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Technology Process of 4-{[1-(3-bromo-phenyl)-meth-(E)-ylidene]-amino}-benzoic acid methyl ester

There total 1 articles about 4-{[1-(3-bromo-phenyl)-meth-(E)-ylidene]-amino}-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 3132-99-8
m-bromobenzoic aldehyde

: 619-45-4
4-methoxycarbonyl aniline

: 1391608-87-9
4-{[1-(3-bromo-phenyl)-meth-(E)-ylidene]-amino}-benzoic acid methyl ester

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 12h; Reflux;

Reference yield: 40.0%

: 1528-30-9
methylenecyclopentane

: 1391608-87-9
4-{[1-(3-bromo-phenyl)-meth-(E)-ylidene]-amino}-benzoic acid methyl ester

: 1391608-88-0
2'-(3-bromo-phenyl)-2',3'-dihydro-1'H-spiro[cyclopentane-1,4'-quinoline]-6'-carboxylic acid methyl ester

Guidance literature:: With scandium tris(trifluoromethanesulfonate); In acetonitrile; at 80 ℃; for 16h; sealed tube;

Reference yield:

: 1391608-87-9
4-{[1-(3-bromo-phenyl)-meth-(E)-ylidene]-amino}-benzoic acid methyl ester

: 1391608-86-8
N-(methylsulfonyl)-2'-(3-morpholinophenyl)-2',3'-dihydro-1'H-spiro[cyclopentane-1,4'-quinoline]-6'-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: scandium tris(trifluoromethanesulfonate) / acetonitrile / 16 h / 80 °C / sealed tube

2.1: potassium carbonate; copper(l) iodide; N,N-dimethylglycine hydrochoride / dimethyl sulfoxide / 16 h / 120 °C

3.1: sodium hydroxide / tetrahydrofuran; methanol / 6 h / 80 °C

3.2: pH 4

4.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 25 °C

4.2: 2 h / 25 - 70 °C

With copper(l) iodide; N,N-dimethylglycine hydrochoride; sodium hydride; potassium carbonate; sodium hydroxide; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; methanol; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;