N-[3-(4,5-dihydropyrazolo[1,5-a]pyrimidin-7-yl)phenyl]-3-(trifluoromethyl)benzamide

Base Information

Chemical Name:N-[3-(4,5-dihydropyrazolo[1,5-a]pyrimidin-7-yl)phenyl]-3-(trifluoromethyl)benzamide
CAS No.:950194-99-7
Molecular Formula:C₂₀H₁₅F₃N₄O
Molecular Weight:384.361
Hs Code.:

Synonyms:N-[3-(4,5-dihydropyrazolo[1,5-a]pyrimidin-7-yl)phenyl]-3-(trifluoromethyl)benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[3-(4,5-dihydropyrazolo[1,5-a]pyrimidin-7-yl)phenyl]-3-(trifluoromethyl)benzamide

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Technology Process of N-[3-(4,5-dihydropyrazolo[1,5-a]pyrimidin-7-yl)phenyl]-3-(trifluoromethyl)benzamide

There total 1 articles about N-[3-(4,5-dihydropyrazolo[1,5-a]pyrimidin-7-yl)phenyl]-3-(trifluoromethyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 950195-00-3
N-(3-pyrazolo[1,5-a]pyrimidin-7-ylphenyl)-3-(trifluoromethyl)benzamide

: 950194-99-7
N-[3-(4,5-dihydropyrazolo[1,5-a]pyrimidin-7-yl)phenyl]-3-(trifluoromethyl)benzamide

Guidance literature:: N-(3-pyrazolo[1,5-a]pyrimidin-7-ylphenyl)-3-(trifluoromethyl)benzamide; With sodium cyanoborohydride; In acetic acid; at 20 ℃; for 2h;

With water; sodium hydrogencarbonate; In ethyl acetate;

Reference yield: 49.0%

: 950194-99-7
N-[3-(4,5-dihydropyrazolo[1,5-a]pyrimidin-7-yl)phenyl]-3-(trifluoromethyl)benzamide

: 124-63-0
methanesulfonyl chloride

: N-{3-[4-(methylsulfonyl)-4,5-dihydropyrazolo[1,5-a]pyrimidin-7-yl]phenyl}-3-(trifluoromethyl)benzamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield: 44.0%

: 950194-99-7
N-[3-(4,5-dihydropyrazolo[1,5-a]pyrimidin-7-yl)phenyl]-3-(trifluoromethyl)benzamide

: 24424-99-5
di-tert-butyl dicarbonate

: 950195-11-6
tert-butyl 7-(3-{(tert-butoxycarbonyl)-[3-(trifluoromethyl)benzoyl]amino}phenyl)pyrazolo[1,5-a]pyrimidine-4(5H)-carboxylate

Guidance literature:: N-[3-(4,5-dihydropyrazolo[1,5-a]pyrimidin-7-yl)phenyl]-3-(trifluoromethyl)benzamide; di-tert-butyl dicarbonate; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃;

With water; In ethyl acetate;