Technology Process of C34H31BrN2
There total 9 articles about C34H31BrN2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bromine; sodium acetate;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 2.5h;
Inert atmosphere;
Darkness;
DOI:10.1002/chem.201304256
- Guidance literature:
-
Multi-step reaction with 5 steps
1: bromine; sodium acetate / tetrahydrofuran / 2.5 h / 0 - 20 °C / Inert atmosphere; Darkness
2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water / Inert atmosphere; Reflux
3: bromine; sodium acetate / tetrahydrofuran / 2.5 h / 0 - 20 °C / Inert atmosphere; Darkness
4: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water / 96 h / Inert atmosphere; Reflux
5: bromine; sodium acetate / tetrahydrofuran / 2.5 h / 0 - 20 °C / Inert atmosphere; Darkness
With
tetrakis(triphenylphosphine) palladium(0); bromine; sodium acetate; sodium carbonate;
In
tetrahydrofuran; water;
2: |Suzuki Coupling / 4: |Suzuki Coupling;
DOI:10.1002/chem.201304256
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water / Inert atmosphere; Reflux
2: bromine; sodium acetate / tetrahydrofuran / 2.5 h / 0 - 20 °C / Inert atmosphere; Darkness
3: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water / 96 h / Inert atmosphere; Reflux
4: bromine; sodium acetate / tetrahydrofuran / 2.5 h / 0 - 20 °C / Inert atmosphere; Darkness
With
tetrakis(triphenylphosphine) palladium(0); bromine; sodium acetate; sodium carbonate;
In
tetrahydrofuran; water;
1: |Suzuki Coupling / 3: |Suzuki Coupling;
DOI:10.1002/chem.201304256