Technology Process of (3S*,4S*)-1-benzoyloxy-4-benzyloxy-3-hydroxyoctane
There total 7 articles about (3S*,4S*)-1-benzoyloxy-4-benzyloxy-3-hydroxyoctane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
tetrahydrofuran;
for 2h;
Heating;
DOI:10.1248/cpb.39.1866
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 75.9 percent / H2 / 5percent rhodium on alumina / ethyl acetate / 4 h / 5320 Torr
2: 97.7 percent / lithium aluminium hydride / diethyl ether / 2 h / Ambient temperature
3: 78.3 percent / triethylamine / benzene / 6 h / Ambient temperature
4: NaH (60percent oil dispersion) / tetrahydrofuran / 6 h
5: tetrabutylammonium fluoride / tetrahydrofuran / 6 h / Ambient temperature
6: 95.1 percent / pyridine / tetrahydrofuran / 2 h / Ambient temperature
7: 81.9 percent / 10percent HCl / tetrahydrofuran / 2 h / Heating
With
pyridine; hydrogenchloride; lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; hydrogen; sodium hydride; triethylamine;
Rh/Al2O3;
In
tetrahydrofuran; diethyl ether; ethyl acetate; benzene;
DOI:10.1248/cpb.39.1866
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 95.1 percent / pyridine / tetrahydrofuran / 2 h / Ambient temperature
2: 81.9 percent / 10percent HCl / tetrahydrofuran / 2 h / Heating
With
pyridine; hydrogenchloride;
In
tetrahydrofuran;
DOI:10.1248/cpb.39.1866
