α-1-C-((1-(3,3-diphenylpropyl)-1H-1,2,3-triazol-4-yl)-methyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

Base Information

• Chemical Name: α-1-C-((1-(3,3-diphenylpropyl)-1H-1,2,3-triazol-4-yl)-methyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol
• CAS No.: 1624966-40-0
• Molecular Formula: C₄₄H₄₆N₄O₃
• Molecular Weight: 678.874

Synonyms:α-1-C-((1-(3,3-diphenylpropyl)-1H-1,2,3-triazol-4-yl)-methyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

Chemical Property of α-1-C-((1-(3,3-diphenylpropyl)-1H-1,2,3-triazol-4-yl)-methyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

Chemical Property:

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Technology Process of α-1-C-((1-(3,3-diphenylpropyl)-1H-1,2,3-triazol-4-yl)-methyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

There total 2 articles about α-1-C-((1-(3,3-diphenylpropyl)-1H-1,2,3-triazol-4-yl)-methyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

α-1-C-propargyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol (1624966-39-7) + 1-azido-3,3-diphenylpropane → α-1-C-((1-(3,3-diphenylpropyl)-1H-1,2,3-triazol-4-yl)-methyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol (1624966-40-0)

Guidance literature:

With copper(ll) sulfate pentahydrate; Erythorbic acid; In tetrahydrofuran; water; at 20 ℃; for 15h;

DOI:10.1002/cmdc.201402023

Reference yield:

α-1-C-propargyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-tert-butoxycarboxylimino-D-xylitol (1624966-37-5) → α-1-C-((1-(3,3-diphenylpropyl)-1H-1,2,3-triazol-4-yl)-methyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol (1624966-40-0)

Guidance literature:

Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

2: copper(ll) sulfate pentahydrate; Erythorbic acid / tetrahydrofuran; water / 15 h / 20 °C

With copper(ll) sulfate pentahydrate; Erythorbic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water;

DOI:10.1002/cmdc.201402023

Reference yield: 80.0%

α-1-C-((1-(3,3-diphenylpropyl)-1H-1,2,3-triazol-4-yl)-methyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol (1624966-40-0) → α-1-C-((1-(3,3-diphenylpropyl)-1H-1,2,3-triazol-4-yl)methyl)-1,5-dideoxy-1,5-imino-D-xylitol (1624966-44-4)

Guidance literature:

With boron trichloride; In dichloromethane; at -60 - 20 ℃; for 16h;

DOI:10.1002/cmdc.201402023

upstream raw materials:

α-1-C-propargyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-tert-butoxycarboxylimino-D-xylitol

α-1-C-propargyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

Downstream raw materials:

α-1-C-((1-(3,3-diphenylpropyl)-1H-1,2,3-triazol-4-yl)methyl)-1,5-dideoxy-1,5-imino-D-xylitol

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