(2-Chloro-phenyl)-(7-nitro-2,3-dihydro-benzo[1,4]dioxin-6-yl)-methanone

Base Information

Chemical Name:(2-Chloro-phenyl)-(7-nitro-2,3-dihydro-benzo[1,4]dioxin-6-yl)-methanone
CAS No.:164526-11-8
Molecular Formula:C₁₅H₁₀ClNO₅
Molecular Weight:319.701
Hs Code.:
DSSTox Substance ID:DTXSID701163426

Synonyms:Oprea1_331327;Oprea1_447235;DTXSID701163426;STK028083;(2-Chloro-phenyl)-(7-nitro-2,3-dihydro-benzo[1,4]dioxin-6-yl)-methanone;AKOS000520064;SR-01000404101;SR-01000404101-1;(2-Chlorophenyl)(2,3-dihydro-7-nitro-1,4-benzodioxin-6-yl)methanone;(2-chlorophenyl)(7-nitro-2,3-dihydro-1,4-benzodioxin-6-yl)methanone;164526-11-8

Suppliers and Price of (2-Chloro-phenyl)-(7-nitro-2,3-dihydro-benzo[1,4]dioxin-6-yl)-methanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-Chloro-phenyl)-(7-nitro-2,3-dihydro-benzo[1,4]dioxin-6-yl)-methanone

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:319.0247501
Heavy Atom Count:22
Complexity:440

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1COC2=C(O1)C=C(C(=C2)[N+](=O)[O-])C(=O)C3=CC=CC=C3Cl

Technology Process of (2-Chloro-phenyl)-(7-nitro-2,3-dihydro-benzo[1,4]dioxin-6-yl)-methanone

There total 1 articles about (2-Chloro-phenyl)-(7-nitro-2,3-dihydro-benzo[1,4]dioxin-6-yl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 164526-07-2
6-(2-chlorobenzoyl)-1,4-benzodioxane

: 164526-11-8
6-(2-chlorobenzoyl)-7-nitro-1,4-benzodioxane

Guidance literature:: With sulfuric acid; nitric acid; In acetic acid; at 10 - 20 ℃; for 1h;
DOI:10.1007/BF01169826

Reference yield: 71.0%

: 164526-11-8
6-(2-chlorobenzoyl)-7-nitro-1,4-benzodioxane

: 164526-16-3
7-amino-2,3-dihydro-1,4-benzodioxin-6-yl 2-chlorophenyl ketone

Guidance literature:: With hydrogenchloride; iron; In ethanol; at 78 ℃; for 6h;
DOI:10.1007/BF01169826

Reference yield:

: 164526-11-8
6-(2-chlorobenzoyl)-7-nitro-1,4-benzodioxane

: 164526-21-0
7-bromoacetamide-6-(2-chlorobenzoyl)-1,4-benzodioxane

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / Fe, HCl / ethanol / 6 h / 78 °C

2: 64 percent / 3N NaOH / dioxane / 2 h / 10 °C

With hydrogenchloride; sodium hydroxide; iron; In 1,4-dioxane; ethanol;
DOI:10.1007/BF01169826