C₁₅H₂₀ClNO₄

Base Information

Chemical Name:C₁₅H₂₀ClNO₄
CAS No.:1256842-57-5
Molecular Formula:C₁₅H₂₀ClNO₄
Molecular Weight:313.781
Hs Code.:

C<sub>15</sub>H<sub>20</sub>ClNO<sub>4</sub>

Synonyms:C₁₅H₂₀ClNO₄

Suppliers and Price of C₁₅H₂₀ClNO₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₅H₂₀ClNO₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₅H₂₀ClNO₄

There total 4 articles about C₁₅H₂₀ClNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1256638-99-9
C₂₃H₂₈ClNO₅

: 1256842-57-5
C₁₅H₂₀ClNO₄

: 437742-34-2
salinosporamide A

Guidance literature:: With ammonium cerium (IV) nitrate; water; In methanol; at 0 ℃; for 6h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/jo101638r

Reference yield:

: C₂₄H₂₆ClNO₅

: 1256842-57-5
C₁₅H₂₀ClNO₄

: 437742-34-2
salinosporamide A

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium on carbon; hydrogen / tetrahydrofuran / 12 h / 23 °C

2.1: dichloro-acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dimethyl sulfoxide; toluene / 6 h / 23 °C / Inert atmosphere

3.1: n-butyllithium; zinc(II) chloride / Inert atmosphere

3.2: Inert atmosphere

4.1: ammonium cerium (IV) nitrate; water / methanol / 6 h / 0 °C / Inert atmosphere

With dichloro-acetic acid; n-butyllithium; ammonium cerium (IV) nitrate; palladium on carbon; water; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; zinc(II) chloride; In tetrahydrofuran; methanol; dimethyl sulfoxide; toluene; 2.1: Moffatt oxidation;
DOI:10.1021/jo101638r

Reference yield:

: 1239897-07-4
C₁₇H₂₀ClNO₅

: 1256842-57-5
C₁₅H₂₀ClNO₄

: 437742-34-2
salinosporamide A

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloro-acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dimethyl sulfoxide; toluene / 6 h / 23 °C / Inert atmosphere

2.1: n-butyllithium; zinc(II) chloride / Inert atmosphere

2.2: Inert atmosphere

3.1: ammonium cerium (IV) nitrate; water / methanol / 6 h / 0 °C / Inert atmosphere

With dichloro-acetic acid; n-butyllithium; ammonium cerium (IV) nitrate; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; zinc(II) chloride; In methanol; dimethyl sulfoxide; toluene; 1.1: Moffatt oxidation;
DOI:10.1021/jo101638r