{[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]methylene}-1,1-diphenylmethanamine

Base Information

Chemical Name:{[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]methylene}-1,1-diphenylmethanamine
CAS No.:1301239-46-2
Molecular Formula:C₁₉H₂₁NO₂
Molecular Weight:295.381
Hs Code.:

Synonyms:{[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]methylene}-1,1-diphenylmethanamine

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Chemical Property of {[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]methylene}-1,1-diphenylmethanamine

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Technology Process of {[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]methylene}-1,1-diphenylmethanamine

There total 3 articles about {[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]methylene}-1,1-diphenylmethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.7%

: 91-00-9
Benzhydrylamine

: 22323-80-4
(4S)-2,2-dimethyl-[1,3]dioxolane-4-carbaldehyde

: 1301239-46-2
{[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]methylene}-1,1-diphenylmethanamine

Guidance literature:: With magnesium sulfate; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1055/s-0030-1258407

Reference yield:

: 98733-24-5
calcium bis[(2R)-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl](hydroxy)acetate]

: 1301239-46-2
{[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]methylene}-1,1-diphenylmethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: calcium hypochlorite; sodium acetate; acetic acid / water / 0.58 h / 50 °C

2: magnesium sulfate / dichloromethane / 0.5 h / 20 °C

With calcium hypochlorite; sodium acetate; magnesium sulfate; acetic acid; In dichloromethane; water;
DOI:10.1055/s-0030-1258407

Reference yield:

: 15042-01-0
5,6-O-isopropylidene-L-ascorbic acid

: 1301239-46-2
{[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]methylene}-1,1-diphenylmethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: dihydrogen peroxide; calcium carbonate / water / 4 h / 20 - 50 °C

2: calcium hypochlorite; sodium acetate; acetic acid / water / 0.58 h / 50 °C

3: magnesium sulfate / dichloromethane / 0.5 h / 20 °C

With calcium hypochlorite; dihydrogen peroxide; sodium acetate; magnesium sulfate; acetic acid; calcium carbonate; In dichloromethane; water;
DOI:10.1055/s-0030-1258407