(+/-)-3,3,6,6,9,9-hexamethyl-12-phenyl-1-oxa-4,7,10-triazacyclododecan-2,5,8,11-tetron

Base Information

Chemical Name:(+/-)-3,3,6,6,9,9-hexamethyl-12-phenyl-1-oxa-4,7,10-triazacyclododecan-2,5,8,11-tetron
CAS No.:87866-96-4
Molecular Formula:C₂₀H₂₇N₃O₅
Molecular Weight:389.451
Hs Code.:

Synonyms:(+/-)-3,3,6,6,9,9-hexamethyl-12-phenyl-1-oxa-4,7,10-triazacyclododecan-2,5,8,11-tetron

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Chemical Property of (+/-)-3,3,6,6,9,9-hexamethyl-12-phenyl-1-oxa-4,7,10-triazacyclododecan-2,5,8,11-tetron

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Technology Process of (+/-)-3,3,6,6,9,9-hexamethyl-12-phenyl-1-oxa-4,7,10-triazacyclododecan-2,5,8,11-tetron

There total 6 articles about (+/-)-3,3,6,6,9,9-hexamethyl-12-phenyl-1-oxa-4,7,10-triazacyclododecan-2,5,8,11-tetron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 87872-95-5
(+/-)-2-<2-<2-(2-hydroxy-2-phenylacetamido)-2-methylpropionamido>-2-methylpropionamido>-N,N,2-trimethylpropionamid

: 87866-96-4
(+/-)-3,3,6,6,9,9-hexamethyl-12-phenyl-1-oxa-4,7,10-triazacyclododecan-2,5,8,11-tetron

Guidance literature:: With hydrogenchloride; In toluene; at 100 ℃;
DOI:10.1002/hlca.19870700209

Reference yield:

: 111492-26-3
(+/-)-2-(2-hydroxy-2-phenylacetamido)-2-methylpropionsaure

: 87866-96-4
(+/-)-3,3,6,6,9,9-hexamethyl-12-phenyl-1-oxa-4,7,10-triazacyclododecan-2,5,8,11-tetron

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / acetonitrile / 2 h / Ambient temperature

2: 85 percent / HCl / toluene / 0.08 h / 100 °C

3: acetonitrile; H₂O / Ambient temperature

4: 91 percent / acetonitrile / 2 h / Ambient temperature

5: 90 percent / HCl / toluene / 100 °C

With hydrogenchloride; In water; toluene; acetonitrile;
DOI:10.1002/hlca.19870700209

Reference yield:

: 87866-93-1
(+/-)-2-<2-(2-hydroxy-2-phenylacetamido)-2-methylpropionamido>-N,N,2-trimethylpropionamid

: 87866-96-4
(+/-)-3,3,6,6,9,9-hexamethyl-12-phenyl-1-oxa-4,7,10-triazacyclododecan-2,5,8,11-tetron

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / HCl / toluene / 0.08 h / 100 °C

2: acetonitrile; H₂O / Ambient temperature

3: 91 percent / acetonitrile / 2 h / Ambient temperature

4: 90 percent / HCl / toluene / 100 °C

With hydrogenchloride; In water; toluene; acetonitrile;
DOI:10.1002/hlca.19870700209