C₅₅H₇₅NO₇S₆

Base Information

Chemical Name:C₅₅H₇₅NO₇S₆
CAS No.:1443384-37-9
Molecular Formula:C₅₅H₇₅NO₇S₆
Molecular Weight:1054.6
Hs Code.:

C<sub>55</sub>H<sub>75</sub>NO<sub>7</sub>S<sub>6</sub>

Synonyms:C₅₅H₇₅NO₇S₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₅H₇₅NO₇S₆

Chemical Property:

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Technology Process of C₅₅H₇₅NO₇S₆

There total 5 articles about C₅₅H₇₅NO₇S₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 62938-08-3
3,5-di-tert-butylbenzyl bromide

: 1443384-36-8
C₄₀H₅₃NO₇S₆

: 1443384-37-9
C₅₅H₇₅NO₇S₆

Guidance literature:: C₄₀H₅₃NO₇S₆; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.25h; Inert atmosphere;

3,5-di-tert-butylbenzyl bromide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1039/c3cc42201a

Reference yield:

: 224298-61-7
1,4-bis[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]benzene monotosylate

: 1443384-37-9
C₅₅H₇₅NO₇S₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium iodide / acetone / 27 h / Inert atmosphere; Reflux

2.1: potassium carbonate / N,N-dimethyl-formamide / 14 h / Inert atmosphere; Reflux

3.1: sodium hydroxide / tetrahydrofuran; water / 0 - 20 °C

4.1: sodium iodide / acetone / 19 h / Inert atmosphere; Reflux

5.1: cesiumhydroxide monohydrate / tetrahydrofuran; methanol / 26 h / 20 °C / Inert atmosphere

5.2: 0.5 h / Inert atmosphere; Reflux

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 20 °C / Inert atmosphere

6.2: 0.25 h / 20 °C / Inert atmosphere

With cesiumhydroxide monohydrate; sodium hydride; potassium carbonate; sodium iodide; sodium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetone; mineral oil;
DOI:10.1039/c3cc42201a

Reference yield:

: 1443384-32-4
C₁₈H₂₉IO₇

: 1443384-37-9
C₅₅H₇₅NO₇S₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 14 h / Inert atmosphere; Reflux

2.1: sodium hydroxide / tetrahydrofuran; water / 0 - 20 °C

3.1: sodium iodide / acetone / 19 h / Inert atmosphere; Reflux

4.1: cesiumhydroxide monohydrate / tetrahydrofuran; methanol / 26 h / 20 °C / Inert atmosphere

4.2: 0.5 h / Inert atmosphere; Reflux

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 20 °C / Inert atmosphere

5.2: 0.25 h / 20 °C / Inert atmosphere

With cesiumhydroxide monohydrate; sodium hydride; potassium carbonate; sodium iodide; sodium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetone; mineral oil;
DOI:10.1039/c3cc42201a