2-(4-methoxyanilino)-3,4,5,6,2',3',4',5',6'-nonafluorobenzophenone

Base Information

• Chemical Name: 2-(4-methoxyanilino)-3,4,5,6,2',3',4',5',6'-nonafluorobenzophenone
• CAS No.: 1299484-35-7
• Molecular Formula: C₂₀H₈F₉NO₂
• Molecular Weight: 465.275
• Mol file: 1299484-35-7.mol

Synonyms:2-(4-methoxyanilino)-3,4,5,6,2',3',4',5',6'-nonafluorobenzophenone

Chemical Property of 2-(4-methoxyanilino)-3,4,5,6,2',3',4',5',6'-nonafluorobenzophenone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(4-methoxyanilino)-3,4,5,6,2',3',4',5',6'-nonafluorobenzophenone

There total 1 articles about 2-(4-methoxyanilino)-3,4,5,6,2',3',4',5',6'-nonafluorobenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

bis(pentafluorophenyl)-methanone (853-39-4) + 4-methoxy-aniline (104-94-9) → 2-(4-methoxyanilino)-3,4,5,6,2',3',4',5',6'-nonafluorobenzophenone (1299484-35-7)

Guidance literature:

In 1,2-dichloro-ethane; at 87 ℃; for 14h; regioselective reaction;

DOI:10.1002/ejoc.201001647

Reference yield: 89.0%

2-(4-methoxyanilino)-3,4,5,6,2',3',4',5',6'-nonafluorobenzophenone (1299484-35-7) → 1,2,3,4-tetrafluoro-7-methoxy-9-pentafluorophenylacridine (1299484-43-7)

Guidance literature:

With sulfuric acid; at 25 ℃; for 24h; Inert atmosphere;

DOI:10.1002/ejoc.201001647

Reference yield: 67.0%

2-(4-methoxyanilino)-3,4,5,6,2',3',4',5',6'-nonafluorobenzophenone (1299484-35-7) → 2-amino-3,4,5,6,2',3',4',5',6'-nonafluorobenzophenone (32962-22-4)

Guidance literature:

With ammonium cerium (IV) nitrate; In water; acetonitrile; at 0 - 25 ℃; for 48h; Inert atmosphere;

DOI:10.1002/ejoc.201001647

upstream raw materials:

bis(pentafluorophenyl)-methanone

4-methoxy-aniline

Downstream raw materials:

1,2,3,4-tetrafluoro-7-methoxy-9-pentafluorophenylacridine

1,2,3,4,5,6,7,8-octafluoro-N-(4-methoxyphenyl)acridone

2-amino-3,4,5,6,2',3',4',5',6'-nonafluorobenzophenone