(S)-1-benzyl 5-(2-(4-(benzyloxycarbonylamino)benzoyloxy)ethyl) 2-(9H-carbazol-9-yl)pentanedioate

Base Information

• Chemical Name: (S)-1-benzyl 5-(2-(4-(benzyloxycarbonylamino)benzoyloxy)ethyl) 2-(9H-carbazol-9-yl)pentanedioate
• CAS No.: 1351464-53-3
• Molecular Formula: C₄₁H₃₆N₂O₈
• Molecular Weight: 684.745
• Mol file: 1351464-53-3.mol

Synonyms:(S)-1-benzyl 5-(2-(4-(benzyloxycarbonylamino)benzoyloxy)ethyl) 2-(9H-carbazol-9-yl)pentanedioate

Chemical Property of (S)-1-benzyl 5-(2-(4-(benzyloxycarbonylamino)benzoyloxy)ethyl) 2-(9H-carbazol-9-yl)pentanedioate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S)-1-benzyl 5-(2-(4-(benzyloxycarbonylamino)benzoyloxy)ethyl) 2-(9H-carbazol-9-yl)pentanedioate

There total 4 articles about (S)-1-benzyl 5-(2-(4-(benzyloxycarbonylamino)benzoyloxy)ethyl) 2-(9H-carbazol-9-yl)pentanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + 4-(benzoyloxycarbonylamino)benzoic acid + (S)-1-benzyl 5-(2-hydroxyethyl) 2-(9H-carbazol-9-yl)pentanedioate (1351464-52-2) + 4-(((benzyloxy)carbonyl)amino)benzoic acid (5330-71-2) + 1,2-dichloro-ethane (107-06-2,52399-93-6) → (S)-1-benzyl 5-(2-(4-(benzyloxycarbonylamino)benzoyloxy)ethyl) 2-(9H-carbazol-9-yl)pentanedioate (1351464-53-3)

Guidance literature:

With dmap; In dichloromethane;

Reference yield:

4-amino-benzoic acid (150-13-0,159246-81-8,8014-65-1) → (S)-1-benzyl 5-(2-(4-(benzyloxycarbonylamino)benzoyloxy)ethyl) 2-(9H-carbazol-9-yl)pentanedioate (1351464-53-3)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / water

2: dmap / dichloromethane

With dmap; sodium hydroxide; In dichloromethane; water;

Reference yield:

(S)-5-(benzyloxy)-4-(9H-carbazol-9-yl)-5-oxopentanoic acid (883977-43-3) → (S)-1-benzyl 5-(2-(4-(benzyloxycarbonylamino)benzoyloxy)ethyl) 2-(9H-carbazol-9-yl)pentanedioate (1351464-53-3)

Guidance literature:

Multi-step reaction with 2 steps

1: dmap / dichloromethane; methanol; ethylene glycol

2: dmap / dichloromethane

With dmap; In methanol; dichloromethane; ethylene glycol;

upstream raw materials:

4-amino-benzoic acid

benzyl chloroformate

hydrogenchloride

(S)-1-benzyl 5-(2-hydroxyethyl) 2-(9H-carbazol-9-yl)pentanedioate

Downstream raw materials:

(S)-5-(2-(4-aminobenzoyloxy)ethoxy)-2-(9H-carbazol-9-yl)-5-oxopentanoic acid