(1S,2R,3R,4S,5R)-2-Amino-3,4,5-tris-benzyloxy-3-benzyloxymethyl-cyclopentanol

Base Information

Chemical Name:(1S,2R,3R,4S,5R)-2-Amino-3,4,5-tris-benzyloxy-3-benzyloxymethyl-cyclopentanol
CAS No.:158631-96-0
Molecular Formula:C₃₄H₃₇NO₅
Molecular Weight:539.671
Hs Code.:

Synonyms:(1S,2R,3R,4S,5R)-2-Amino-3,4,5-tris-benzyloxy-3-benzyloxymethyl-cyclopentanol

Suppliers and Price of (1S,2R,3R,4S,5R)-2-Amino-3,4,5-tris-benzyloxy-3-benzyloxymethyl-cyclopentanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R,3R,4S,5R)-2-Amino-3,4,5-tris-benzyloxy-3-benzyloxymethyl-cyclopentanol

Chemical Property:

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Technology Process of (1S,2R,3R,4S,5R)-2-Amino-3,4,5-tris-benzyloxy-3-benzyloxymethyl-cyclopentanol

There total 10 articles about (1S,2R,3R,4S,5R)-2-Amino-3,4,5-tris-benzyloxy-3-benzyloxymethyl-cyclopentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 158632-02-1
(3aR,4R,5S,6R,6aS)-4,5,6-Tris-benzyloxy-4-benzyloxymethyl-hexahydro-cyclopentaoxazol-2-one

: 158631-96-0
(1S,2R,3R,4S,5R)-2-Amino-3,4,5-tris-benzyloxy-3-benzyloxymethyl-cyclopentanol

Guidance literature:: With potassium hydroxide; In ethanol; for 12h; Heating;

Reference yield:

: 89291-76-9
(1S,4R,5S)-(-)-3-<(benzyloxy)methyl>-4,5-O-isopropylidene-2-cyclopenten-1-ol

: 158631-96-0
(1S,2R,3R,4S,5R)-2-Amino-3,4,5-tris-benzyloxy-3-benzyloxymethyl-cyclopentanol

Guidance literature:: Multi-step reaction with 10 steps

1: 1.) NaH, MeI, 2.) I₂, Na₂CO₃, Na₂SO₃ / 2.) THF

2: 1.) H₂SO₄, 2.) Zn / 2.) THF

3: K₂CO₃ / methanol; H₂O

4: DEAD, Ph₃P / toluene

5: Na₂CO₃, H₂O / methanol

6: 90 percent / CF₃CO₃H, Na₂CO₃ / CH₂Cl₂ / -20 °C

7: 89 percent / PhCO₂Na, H₂O / dimethylformamide / 12 h / 100 °C

8: NaH, n-Bu₄NI / tetrahydrofuran

9: CAN / acetonitrile; H₂O

10: 2 N aq. KOH / ethanol / 12 h / Heating

With sodium benzoate; potassium hydroxide; ammonium cerium(IV) nitrate; trifluoroacetyl peroxide; sulfuric acid; water; iodine; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium carbonate; potassium carbonate; triphenylphosphine; sodium sulfite; zinc; diethylazodicarboxylate; methyl iodide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 158632-00-9
(1aR,1bR,4aS,5R,5aR)-1a-Benzyloxymethyl-5-hydroxy-2-(4-methoxy-benzyl)-hexahydro-1,4-dioxa-2-aza-cyclopropa[a]pentalen-3-one

: 158631-96-0
(1S,2R,3R,4S,5R)-2-Amino-3,4,5-tris-benzyloxy-3-benzyloxymethyl-cyclopentanol

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / PhCO₂Na, H₂O / dimethylformamide / 12 h / 100 °C

2: NaH, n-Bu₄NI / tetrahydrofuran

3: CAN / acetonitrile; H₂O

4: 2 N aq. KOH / ethanol / 12 h / Heating

With sodium benzoate; potassium hydroxide; ammonium cerium(IV) nitrate; water; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; acetonitrile;