(3R,4R,5R,6R)-N-benzyloxycarbonyl-3-hydroxy-4,5,6-tribenzyloxyazepane

Base Information

Chemical Name:(3R,4R,5R,6R)-N-benzyloxycarbonyl-3-hydroxy-4,5,6-tribenzyloxyazepane
CAS No.:1357280-99-9
Molecular Formula:C₃₅H₃₇NO₆
Molecular Weight:567.682
Hs Code.:

Synonyms:(3R,4R,5R,6R)-N-benzyloxycarbonyl-3-hydroxy-4,5,6-tribenzyloxyazepane

Suppliers and Price of (3R,4R,5R,6R)-N-benzyloxycarbonyl-3-hydroxy-4,5,6-tribenzyloxyazepane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,4R,5R,6R)-N-benzyloxycarbonyl-3-hydroxy-4,5,6-tribenzyloxyazepane

Chemical Property:

Purity/Quality:

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Technology Process of (3R,4R,5R,6R)-N-benzyloxycarbonyl-3-hydroxy-4,5,6-tribenzyloxyazepane

There total 9 articles about (3R,4R,5R,6R)-N-benzyloxycarbonyl-3-hydroxy-4,5,6-tribenzyloxyazepane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1357280-97-7
(3R,4R,5R,6R)-3-hydroxy-4,5,6-tribenzyloxyazepane

: 501-53-1,94274-21-2
benzyl chloroformate

: 1357280-99-9
(3R,4R,5R,6R)-N-benzyloxycarbonyl-3-hydroxy-4,5,6-tribenzyloxyazepane

Guidance literature:: With potassium hydrogencarbonate; In water; ethyl acetate; at 0 ℃; for 3h;
DOI:10.1016/j.bmc.2010.09.053

Reference yield:

: 51103-66-3
methyl 6-O-(p-tolylsulfonyl)-α-D-mannopyranoside

: 1357280-99-9
(3R,4R,5R,6R)-N-benzyloxycarbonyl-3-hydroxy-4,5,6-tribenzyloxyazepane

Guidance literature:: Multi-step reaction with 7 steps

1: sodium azide / N,N-dimethyl-formamide

2: sodium hydride / N,N-dimethyl-formamide

3: sulfuric acid / dichloromethane / 0.08 h / -10 °C

4: sodium methylate / methanol / 1 h / 20 °C

5: triphenylphosphine / tetrahydrofuran

6: sodium cyanoborohydride; acetic acid

7: potassium hydrogencarbonate / water; ethyl acetate / 3 h / 0 °C

With sodium azide; sulfuric acid; sodium methylate; sodium hydride; sodium cyanoborohydride; potassium hydrogencarbonate; acetic acid; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2010.09.053

Reference yield:

: 66224-56-4
methyl 6-azido-6-deoxy-α-D-mannopyranoside

: 1357280-99-9
(3R,4R,5R,6R)-N-benzyloxycarbonyl-3-hydroxy-4,5,6-tribenzyloxyazepane

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydride / N,N-dimethyl-formamide

2: sulfuric acid / dichloromethane / 0.08 h / -10 °C

3: sodium methylate / methanol / 1 h / 20 °C

4: triphenylphosphine / tetrahydrofuran

5: sodium cyanoborohydride; acetic acid

6: potassium hydrogencarbonate / water; ethyl acetate / 3 h / 0 °C

With sulfuric acid; sodium methylate; sodium hydride; sodium cyanoborohydride; potassium hydrogencarbonate; acetic acid; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2010.09.053