6t,7t-O-Isopropyliden-1,3-dioxo-2-phenyl-1,3,5,6,7,8-hexahydro<2H>-s-triazolo<1,2-a>pyridazin-5r-carbaldehyd-dimethylacetal

Base Information

Chemical Name:6t,7t-O-Isopropyliden-1,3-dioxo-2-phenyl-1,3,5,6,7,8-hexahydro<2H>-s-triazolo<1,2-a>pyridazin-5r-carbaldehyd-dimethylacetal
CAS No.:75773-28-3
Molecular Formula:C₁₈H₂₃N₃O₆
Molecular Weight:377.397
Hs Code.:

Synonyms:6t,7t-O-Isopropyliden-1,3-dioxo-2-phenyl-1,3,5,6,7,8-hexahydro<2H>-s-triazolo<1,2-a>pyridazin-5r-carbaldehyd-dimethylacetal

Suppliers and Price of 6t,7t-O-Isopropyliden-1,3-dioxo-2-phenyl-1,3,5,6,7,8-hexahydro<2H>-s-triazolo<1,2-a>pyridazin-5r-carbaldehyd-dimethylacetal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6t,7t-O-Isopropyliden-1,3-dioxo-2-phenyl-1,3,5,6,7,8-hexahydro<2H>-s-triazolo<1,2-a>pyridazin-5r-carbaldehyd-dimethylacetal

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6t,7t-O-Isopropyliden-1,3-dioxo-2-phenyl-1,3,5,6,7,8-hexahydro<2H>-s-triazolo<1,2-a>pyridazin-5r-carbaldehyd-dimethylacetal

There total 5 articles about 6t,7t-O-Isopropyliden-1,3-dioxo-2-phenyl-1,3,5,6,7,8-hexahydro<2H>-s-triazolo<1,2-a>pyridazin-5r-carbaldehyd-dimethylacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 75773-25-0
6t,7t-Dihydroxy-1,3-dioxo-2-phenyl-1,3,5,6,7,8-hexahydro<2H>-s-triazolo<1,2-a>pyridazin-5r-carbaldehyd-dimethylacetal

: 67-64-1
acetone

: 75773-28-3
6t,7t-O-Isopropyliden-1,3-dioxo-2-phenyl-1,3,5,6,7,8-hexahydro<2H>-s-triazolo<1,2-a>pyridazin-5r-carbaldehyd-dimethylacetal

Guidance literature:: With Bis(p-nitrophenyl) phosphate; In various solvent(s); for 1.5h; Ambient temperature;

Reference yield:

: 4233-33-4
4-Phenyl-1,2,4-triazolidine-3,5-dione

: 75773-28-3
6t,7t-O-Isopropyliden-1,3-dioxo-2-phenyl-1,3,5,6,7,8-hexahydro<2H>-s-triazolo<1,2-a>pyridazin-5r-carbaldehyd-dimethylacetal

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / CH₂Cl₂ / 1 h / 0 °C

2: 41 percent / OsO₄-catalysatorsolution, 30 percent H₂O₂ / acetone / 72 h / Ambient temperature

3: 90 percent / Bis(p-nitrophenyl)phosphat / various solvent(s) / 1.5 h / Ambient temperature

With osmium(VIII) oxide; Bis(p-nitrophenyl) phosphate; dihydrogen peroxide; In dichloromethane; acetone;

Reference yield:

: 20432-40-0
(E)-penta-2,4-dienal

: 75773-28-3
6t,7t-O-Isopropyliden-1,3-dioxo-2-phenyl-1,3,5,6,7,8-hexahydro<2H>-s-triazolo<1,2-a>pyridazin-5r-carbaldehyd-dimethylacetal

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent

2: 99 percent / CH₂Cl₂ / 1 h / 0 °C

3: 41 percent / OsO₄-catalysatorsolution, 30 percent H₂O₂ / acetone / 72 h / Ambient temperature

4: 90 percent / Bis(p-nitrophenyl)phosphat / various solvent(s) / 1.5 h / Ambient temperature

With osmium(VIII) oxide; Bis(p-nitrophenyl) phosphate; dihydrogen peroxide; In dichloromethane; acetone;