1,2-bis-(2'-methyl-5'-phenylthien-3'-yl)-1,3-dimethyl-2-13C-imidazolium iodide

Base Information

Chemical Name:1,2-bis-(2'-methyl-5'-phenylthien-3'-yl)-1,3-dimethyl-2-13C-imidazolium iodide
CAS No.:1384896-95-0
Molecular Formula:C₂₇H₂₅N₂S₂*I
Molecular Weight:569.534
Hs Code.:

Synonyms:1,2-bis-(2'-methyl-5'-phenylthien-3'-yl)-1,3-dimethyl-2-13C-imidazolium iodide

Suppliers and Price of 1,2-bis-(2'-methyl-5'-phenylthien-3'-yl)-1,3-dimethyl-2-13C-imidazolium iodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,2-bis-(2'-methyl-5'-phenylthien-3'-yl)-1,3-dimethyl-2-13C-imidazolium iodide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,2-bis-(2'-methyl-5'-phenylthien-3'-yl)-1,3-dimethyl-2-13C-imidazolium iodide

There total 1 articles about 1,2-bis-(2'-methyl-5'-phenylthien-3'-yl)-1,3-dimethyl-2-13C-imidazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1384896-94-9
1,2-bis-(2'-methyl-5'-phenylthien-3'-yl)-2-13C-imidazole

: 74-88-4
methyl iodide

: 1384896-95-0
1,2-bis-(2'-methyl-5'-phenylthien-3'-yl)-1,3-dimethyl-2-13C-imidazolium iodide

Guidance literature:: With potassium carbonate; In acetonitrile; at 80 ℃; for 16h;
DOI:10.1021/ja304067k

Reference yield: 86.0%

: 1384896-95-0
1,2-bis-(2'-methyl-5'-phenylthien-3'-yl)-1,3-dimethyl-2-13C-imidazolium iodide

: 1,2-bis-(2'-methyl-5'-phenylthien-3'-yl)-1,3-dimethyl-2-13C-imidazolium hexafluorophosphate

Guidance literature:: With silver(I) hexafluorophosphate; In dichloromethane; at 20 ℃; for 0.25h;
DOI:10.1021/ja304067k

Reference yield:

: 1384896-95-0
1,2-bis-(2'-methyl-5'-phenylthien-3'-yl)-1,3-dimethyl-2-13C-imidazolium iodide

: 1384896-98-3
1,2-bis-(2'-methyl-5'-phenylthien-3'-yl)-1,3-dimethylimidazol-2-13C-ylidene

Guidance literature:: Multi-step reaction with 2 steps

1: silver(I) hexafluorophosphate / dichloromethane / 0.25 h / 20 °C

2: sodium hexamethyldisilazane / C₆D₆ / 0.5 h / 20 °C / Inert atmosphere

With silver(I) hexafluorophosphate; sodium hexamethyldisilazane; In dichloromethane; C₆D₆;
DOI:10.1021/ja304067k