2-cyano-3-(2-iodophenyl)-2-propenethioamide

Base Information

Chemical Name:2-cyano-3-(2-iodophenyl)-2-propenethioamide
CAS No.:161689-29-8
Molecular Formula:C₁₀H₇IN₂S
Molecular Weight:314.149
Hs Code.:

Synonyms:2-cyano-3-(2-iodophenyl)-2-propenethioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-cyano-3-(2-iodophenyl)-2-propenethioamide

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Technology Process of 2-cyano-3-(2-iodophenyl)-2-propenethioamide

There total 1 articles about 2-cyano-3-(2-iodophenyl)-2-propenethioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 7357-70-2
Cyanothioacetamide

: 26260-02-6
2-iodobenzaldehyde

: 161689-29-8
2-cyano-3-(2-iodophenyl)-2-propenethioamide

Guidance literature:: With piperidine; In 1,4-dioxane; at 80 ℃;
DOI:10.1021/jm301575n

Reference yield: 43.0%

: 161689-29-8
2-cyano-3-(2-iodophenyl)-2-propenethioamide

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1286771-75-2
4-(2-iodophenyl)-2-thioxo-1,2,5,6,7,8-hexahydroquinoline-3-carbonitrile

Guidance literature:: With piperidine; In 1,4-dioxane; at 80 ℃; for 2h;
DOI:10.1021/jm301575n

Reference yield:

: 161689-29-8
2-cyano-3-(2-iodophenyl)-2-propenethioamide

: 1286771-54-7
[3-amino-4-(2-iodophenyl)-5,6,7,8-tetrahydrothieno[2,3-b]quinoline-2-yl](phenyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / 1,4-dioxane / 2 h / 80 °C

2: potassium hydroxide / N,N-dimethyl-formamide; water / 0.83 h / 20 °C / Enzymatic reaction

With piperidine; potassium hydroxide; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm301575n