N-(2-bromophenyl)-N-methyl-2-(acetylamino)-4-chlorobenzenesulfonamide

Base Information

Chemical Name:N-(2-bromophenyl)-N-methyl-2-(acetylamino)-4-chlorobenzenesulfonamide
CAS No.:132749-70-3
Molecular Formula:C₁₅H₁₄BrClN₂O₃S
Molecular Weight:417.711
Hs Code.:

Synonyms:N-(2-bromophenyl)-N-methyl-2-(acetylamino)-4-chlorobenzenesulfonamide

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Chemical Property of N-(2-bromophenyl)-N-methyl-2-(acetylamino)-4-chlorobenzenesulfonamide

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Technology Process of N-(2-bromophenyl)-N-methyl-2-(acetylamino)-4-chlorobenzenesulfonamide

There total 4 articles about N-(2-bromophenyl)-N-methyl-2-(acetylamino)-4-chlorobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 132749-61-2
N-(2-bromophenyl)-2-(acetylamino)-4-chlorobenzenesulfonamide

: 132749-70-3
N-(2-bromophenyl)-N-methyl-2-(acetylamino)-4-chlorobenzenesulfonamide

Guidance literature:: With sodium methylate; In methanol; for 24h; Ambient temperature;
DOI:10.1021/jm00108a018

Reference yield:

: 4533-96-4
4-chloro-2-nitrobenzenesulfonyl chloride

: 132749-70-3
N-(2-bromophenyl)-N-methyl-2-(acetylamino)-4-chlorobenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / pyridine / tetrahydrofuran / 2 h / Heating

2: iron, acetic acid / 1 h / Heating

3: acetic acid

4: 90 percent / NaOCH₃ / methanol / 24 h / Ambient temperature

With pyridine; sodium methylate; iron; acetic acid; In tetrahydrofuran; methanol;
DOI:10.1021/jm00108a018

Reference yield:

: 1040069-05-3
2-Amino-N-(2-bromo-phenyl)-4-chloro-benzenesulfonamide

: 132749-70-3
N-(2-bromophenyl)-N-methyl-2-(acetylamino)-4-chlorobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid

2: 90 percent / NaOCH₃ / methanol / 24 h / Ambient temperature

With sodium methylate; acetic acid; In methanol;
DOI:10.1021/jm00108a018