acetic acid 1-[2-(1-acetoxy-3-phenyl-prop-2-ynyl)-phenyl]-3-phenyl-prop-2-ynyl ester

Base Information

• Chemical Name: acetic acid 1-[2-(1-acetoxy-3-phenyl-prop-2-ynyl)-phenyl]-3-phenyl-prop-2-ynyl ester
• CAS No.: 141068-40-8
• Molecular Formula: C₂₈H₂₂O₄
• Molecular Weight: 422.48
• Mol file: 141068-40-8.mol

Synonyms:acetic acid 1-[2-(1-acetoxy-3-phenyl-prop-2-ynyl)-phenyl]-3-phenyl-prop-2-ynyl ester

Chemical Property of acetic acid 1-[2-(1-acetoxy-3-phenyl-prop-2-ynyl)-phenyl]-3-phenyl-prop-2-ynyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of acetic acid 1-[2-(1-acetoxy-3-phenyl-prop-2-ynyl)-phenyl]-3-phenyl-prop-2-ynyl ester

There total 4 articles about acetic acid 1-[2-(1-acetoxy-3-phenyl-prop-2-ynyl)-phenyl]-3-phenyl-prop-2-ynyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-[2-(1-hydroxy-3-phenylprop-2-ynyl)phenyl]-3-phenylprop-2-yn-1-ol (36229-69-3) + acetyl chloride (75-36-5) → acetic acid 1-[2-(1-acetoxy-3-phenyl-prop-2-ynyl)-phenyl]-3-phenyl-prop-2-ynyl ester (141068-40-8)

Guidance literature:

With pyridine; dmap; In dichloromethane; at 0 ℃;

DOI:10.1002/adsc.200800037

Reference yield:

o-phthalic dicarboxaldehyde (643-79-8) → acetic acid 1-[2-(1-acetoxy-3-phenyl-prop-2-ynyl)-phenyl]-3-phenyl-prop-2-ynyl ester (141068-40-8)

Guidance literature:

Multi-step reaction with 2 steps

2: DMAP

With dmap;

DOI:10.1016/S0040-4039(00)60926-7

Reference yield:

lithium phenylacetylide (4440-01-1) → acetic acid 1-[2-(1-acetoxy-3-phenyl-prop-2-ynyl)-phenyl]-3-phenyl-prop-2-ynyl ester (141068-40-8)

Guidance literature:

Multi-step reaction with 2 steps

2: DMAP

With dmap;

DOI:10.1016/S0040-4039(00)60926-7

upstream raw materials:

1-[2-(1-hydroxy-3-phenylprop-2-ynyl)phenyl]-3-phenylprop-2-yn-1-ol

acetic anhydride

o-phthalic dicarboxaldehyde

lithium phenylacetylide

Downstream raw materials:

phenyl-(3-phenylethynyl-1H-inden-2-yl)-methanone

cis-1,2-Diphenyl-naphthocyclobuten

trans-1,2-Dihydro-1,2-diphenylcyclobutanaphthalin