selenothiobenzoic acid S-2-(trimethylsilyl)ethyl ester

Base Information

Chemical Name:selenothiobenzoic acid S-2-(trimethylsilyl)ethyl ester
CAS No.:307000-62-0
Molecular Formula:C₁₂H₁₈SSeSi
Molecular Weight:301.386
Hs Code.:

Synonyms:selenothiobenzoic acid S-2-(trimethylsilyl)ethyl ester

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Chemical Property of selenothiobenzoic acid S-2-(trimethylsilyl)ethyl ester

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Technology Process of selenothiobenzoic acid S-2-(trimethylsilyl)ethyl ester

There total 1 articles about selenothiobenzoic acid S-2-(trimethylsilyl)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 18143-30-1
2-trimethylsilylethanethiol

: 5925-76-8
selenobenzoic acid O-methyl ester

: 307000-62-0
selenothiobenzoic acid S-2-(trimethylsilyl)ethyl ester

Guidance literature:: 2-trimethylsilylethanethiol; With trimethylaluminum; In toluene; at -78 ℃; for 1h;

selenobenzoic acid O-methyl ester; In toluene; at 20 ℃; for 3h; Further stages.;
DOI:10.1021/ja000530v

Reference yield:

: 429-41-4
tetrabutyl ammonium fluoride

: 307000-62-0
selenothiobenzoic acid S-2-(trimethylsilyl)ethyl ester

: tetrabutylammonium selenothiobenzoate

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 3h;
DOI:10.1021/ja000530v

Reference yield:

: 307000-62-0
selenothiobenzoic acid S-2-(trimethylsilyl)ethyl ester

: 136970-32-6
selenothiobenzoic acid Se-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 3 h / 0 °C

2: 77 percent / tetrahydrofuran / 1 h / 0 °C

In tetrahydrofuran;
DOI:10.1021/ja000530v