Technology Process of C36H50O2S2
There total 8 articles about C36H50O2S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium tert-butylate;
In
tetrahydrofuran;
at -40 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: dichloromethane / 2 h / 20 °C
2: diisobutylaluminium hydride / dichloromethane / 0.5 h / 0 °C
3: palladium on activated charcoal; hydrogen / 4 h / 20 °C
4: pyridinium chlorochromate / dichloromethane / 10 h / 20 °C
5: dichloromethane / 0.5 h / 20 °C
6: diisobutylaluminium hydride / dichloromethane / 0.33 h / 0 °C
7: triphenylphosphine; carbon tetrabromide / 0.25 h / 0 °C
8: potassium tert-butylate / tetrahydrofuran / 0.5 h / -40 °C
With
carbon tetrabromide; palladium on activated charcoal; potassium tert-butylate; hydrogen; diisobutylaluminium hydride; triphenylphosphine; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: diisobutylaluminium hydride / dichloromethane / 0.5 h / 0 °C
2: palladium on activated charcoal; hydrogen / 4 h / 20 °C
3: pyridinium chlorochromate / dichloromethane / 10 h / 20 °C
4: dichloromethane / 0.5 h / 20 °C
5: diisobutylaluminium hydride / dichloromethane / 0.33 h / 0 °C
6: triphenylphosphine; carbon tetrabromide / 0.25 h / 0 °C
7: potassium tert-butylate / tetrahydrofuran / 0.5 h / -40 °C
With
carbon tetrabromide; palladium on activated charcoal; potassium tert-butylate; hydrogen; diisobutylaluminium hydride; triphenylphosphine; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane;