N-[(2R,4aR,6R,7R,8R,8aS)-6-[8-(4-Methoxy-phenoxy)-octyloxy]-2-phenyl-8-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Base Information

Chemical Name:N-[(2R,4aR,6R,7R,8R,8aS)-6-[8-(4-Methoxy-phenoxy)-octyloxy]-2-phenyl-8-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide
CAS No.:179093-77-7
Molecular Formula:C₃₆H₅₁NO₁₃
Molecular Weight:705.8
Hs Code.:

N-[(2R,4aR,6R,7R,8R,8aS)-6-[8-(4-Methoxy-phenoxy)-octyloxy]-2-phenyl-8-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Synonyms:N-[(2R,4aR,6R,7R,8R,8aS)-6-[8-(4-Methoxy-phenoxy)-octyloxy]-2-phenyl-8-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

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Chemical Property of N-[(2R,4aR,6R,7R,8R,8aS)-6-[8-(4-Methoxy-phenoxy)-octyloxy]-2-phenyl-8-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

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Technology Process of N-[(2R,4aR,6R,7R,8R,8aS)-6-[8-(4-Methoxy-phenoxy)-octyloxy]-2-phenyl-8-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

There total 6 articles about N-[(2R,4aR,6R,7R,8R,8aS)-6-[8-(4-Methoxy-phenoxy)-octyloxy]-2-phenyl-8-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 178986-46-4
N-[(2R,4aR,6R,7R,8R,8aS)-6-[8-(4-Methoxy-phenoxy)-octyloxy]-2-phenyl-8-((2S,3R,4S,5S,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

: 179093-77-7
N-[(2R,4aR,6R,7R,8R,8aS)-6-[8-(4-Methoxy-phenoxy)-octyloxy]-2-phenyl-8-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 12h; Ambient temperature;
DOI:10.1016/0968-0896(96)00064-8

Reference yield:

: 53081-30-4
tetra-O-benzyl-α-D-galactosyl bromide

: 179093-77-7
N-[(2R,4aR,6R,7R,8R,8aS)-6-[8-(4-Methoxy-phenoxy)-octyloxy]-2-phenyl-8-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) silver carbonate, silver triflate, CaSO₄ / 1.) CH₂Cl₂, -25 deg C, 2 h, 2.) CH₂Cl₂, a.) -25 deg C, 3 h, b.) RT, 12 h

2: 90 percent / H₂ / 10percent Pd/C / methanol / 12 h / Ambient temperature

With calcium sulfate; hydrogen; silver trifluoromethanesulfonate; silver carbonate; palladium on activated charcoal; In methanol;
DOI:10.1016/0968-0896(96)00064-8

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 179093-77-7
N-[(2R,4aR,6R,7R,8R,8aS)-6-[8-(4-Methoxy-phenoxy)-octyloxy]-2-phenyl-8-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / p-toluenesulfonic acid / dimethylformamide / 3 h / 60 °C

2: 1.) silver carbonate, silver triflate, CaSO₄ / 1.) CH₂Cl₂, -25 deg C, 2 h, 2.) CH₂Cl₂, a.) -25 deg C, 3 h, b.) RT, 12 h

3: 90 percent / H₂ / 10percent Pd/C / methanol / 12 h / Ambient temperature

With calcium sulfate; hydrogen; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; silver carbonate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/0968-0896(96)00064-8