N-(3,4-methylenedioxyphenyl)methyl-N-(2-phenylsulfinylethyl)-3-methoxyaminobenzene

Base Information

Chemical Name:N-(3,4-methylenedioxyphenyl)methyl-N-(2-phenylsulfinylethyl)-3-methoxyaminobenzene
CAS No.:374593-78-9
Molecular Formula:C₂₃H₂₃NO₄S
Molecular Weight:409.506
Hs Code.:

Synonyms:N-(3,4-methylenedioxyphenyl)methyl-N-(2-phenylsulfinylethyl)-3-methoxyaminobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3,4-methylenedioxyphenyl)methyl-N-(2-phenylsulfinylethyl)-3-methoxyaminobenzene

Chemical Property:

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Technology Process of N-(3,4-methylenedioxyphenyl)methyl-N-(2-phenylsulfinylethyl)-3-methoxyaminobenzene

There total 7 articles about N-(3,4-methylenedioxyphenyl)methyl-N-(2-phenylsulfinylethyl)-3-methoxyaminobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 374593-77-8
N-(3,4-methylenedioxyphenylmethyl)-N-(2-phenylsulfanylethyl)-3-methoxyaminobenzene

: 374593-78-9
N-(3,4-methylenedioxyphenyl)methyl-N-(2-phenylsulfinylethyl)-3-methoxyaminobenzene

Guidance literature:: With sodium periodate; In water; acetone; for 20h; Heating;
DOI:10.1248/cpb.49.1132

Reference yield:

: 7031-27-8
(phenylthio)acetic acid chloride

: 374593-78-9
N-(3,4-methylenedioxyphenyl)methyl-N-(2-phenylsulfinylethyl)-3-methoxyaminobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 22.6 g / Et₃N / benzene / 20 h / 20 °C

2: 84 percent / AlH₃ / tetrahydrofuran; diethyl ether / 0.5 h / 20 °C

3: 82 percent / NaIO₄ / acetone; H₂O / 20 h / Heating

With aluminium hydride; sodium periodate; triethylamine; In tetrahydrofuran; diethyl ether; water; acetone; benzene;
DOI:10.1248/cpb.49.1132

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 374593-78-9
N-(3,4-methylenedioxyphenyl)methyl-N-(2-phenylsulfinylethyl)-3-methoxyaminobenzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: Ti(i-PrO)4 / 3 h / 80 °C

1.2: 99 percent / NaBH₄ / methanol / 1 h / 20 °C

2.1: 22.6 g / Et₃N / benzene / 20 h / 20 °C

3.1: 84 percent / AlH₃ / tetrahydrofuran; diethyl ether / 0.5 h / 20 °C

4.1: 82 percent / NaIO₄ / acetone; H₂O / 20 h / Heating

With aluminium hydride; titanium(IV) isopropylate; sodium periodate; triethylamine; In tetrahydrofuran; diethyl ether; water; acetone; benzene;
DOI:10.1248/cpb.49.1132