2-bromoethyl 2-(phenylmethoxy)-3-(4-tetradecylphenoxy)propyl phosphate

Base Information

Chemical Name:2-bromoethyl 2-(phenylmethoxy)-3-(4-tetradecylphenoxy)propyl phosphate
CAS No.:90857-90-2
Molecular Formula:C₃₂H₅₀BrO₆P
Molecular Weight:641.623
Hs Code.:

Synonyms:2-bromoethyl 2-(phenylmethoxy)-3-(4-tetradecylphenoxy)propyl phosphate

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Chemical Property of 2-bromoethyl 2-(phenylmethoxy)-3-(4-tetradecylphenoxy)propyl phosphate

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Technology Process of 2-bromoethyl 2-(phenylmethoxy)-3-(4-tetradecylphenoxy)propyl phosphate

There total 10 articles about 2-bromoethyl 2-(phenylmethoxy)-3-(4-tetradecylphenoxy)propyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90857-88-8
2-(phenylmethoxy)-3-(4-tetradecylphenoxy)-1-propanol

: 90857-90-2
2-bromoethyl 2-(phenylmethoxy)-3-(4-tetradecylphenoxy)propyl phosphate

Guidance literature:: With hydrogenchloride; sodium acetate; triethylamine; In tetrahydrofuran; tetrachloromethane;

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 90857-90-2
2-bromoethyl 2-(phenylmethoxy)-3-(4-tetradecylphenoxy)propyl phosphate

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) Mg, 2.) dilithium tetrachlorocopper(II) / 1.) THF, reflux, 2 h, 2.) a) THF, reflux, 2 h, b) THF, RT, 16 h

2: 94 percent / BBr₃ / CH₂Cl₂ / 3 h / Ambient temperature

3: 1.) NaH / 1.) DMF, reflux, 2 h, 2.) DMF, reflux, 24 h

4: 95 percent / 1N aq. HCl / methanol / 3 h / Heating

5: 42 percent / pyridine / 48 h / Ambient temperature

6: 99 percent / NaH / dimethylformamide / 3 h / Ambient temperature

7: 80 percent / p-TsOH / methanol; tetrahydrofuran / 24 h / Ambient temperature

8: 1.) Et₃N, 2.) 0.5 M aq. AcONa / 1.) CCl₄, 2 h, 2.) THF

With pyridine; hydrogenchloride; dilithium tetrachlorocuprate; sodium acetate; boron tribromide; sodium hydride; toluene-4-sulfonic acid; magnesium; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00375a016

Reference yield:

: 19218-94-1
1-iodotetradecane

: 90857-90-2
2-bromoethyl 2-(phenylmethoxy)-3-(4-tetradecylphenoxy)propyl phosphate

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) Mg, 2.) dilithium tetrachlorocopper(II) / 1.) THF, reflux, 2 h, 2.) a) THF, reflux, 2 h, b) THF, RT, 16 h

2: 94 percent / BBr₃ / CH₂Cl₂ / 3 h / Ambient temperature

3: 1.) NaH / 1.) DMF, reflux, 2 h, 2.) DMF, reflux, 24 h

4: 95 percent / 1N aq. HCl / methanol / 3 h / Heating

5: 42 percent / pyridine / 48 h / Ambient temperature

6: 99 percent / NaH / dimethylformamide / 3 h / Ambient temperature

7: 80 percent / p-TsOH / methanol; tetrahydrofuran / 24 h / Ambient temperature

8: 1.) Et₃N, 2.) 0.5 M aq. AcONa / 1.) CCl₄, 2 h, 2.) THF

With pyridine; hydrogenchloride; dilithium tetrachlorocuprate; sodium acetate; boron tribromide; sodium hydride; toluene-4-sulfonic acid; magnesium; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00375a016