1-(3,5-di-O-acetyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-5-benzyluracil

Base Information

Chemical Name:1-(3,5-di-O-acetyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-5-benzyluracil
CAS No.:159042-29-2
Molecular Formula:C₂₀H₂₁FN₂O₇
Molecular Weight:420.394
Hs Code.:

Synonyms:1-(3,5-di-O-acetyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-5-benzyluracil

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3,5-di-O-acetyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-5-benzyluracil

Chemical Property:

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Technology Process of 1-(3,5-di-O-acetyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-5-benzyluracil

There total 8 articles about 1-(3,5-di-O-acetyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-5-benzyluracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18493-83-9
5-benzyluracil

: 159042-29-2
1-(3,5-di-O-acetyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-5-benzyluracil

Guidance literature:: Multi-step reaction with 4 steps

1: (NH₄)2SO₄ / 2 h / Heating

2: 55 percent / CH₂Cl₂ / 120 h / Ambient temperature

3: NH₃, MeOH / 48 h / Ambient temperature

4: pyridine

With pyridine; methanol; ammonium sulfate; ammonia; In dichloromethane;
DOI:10.1080/15257779408013228

Reference yield:

: 5909-45-5
5-benzylpyrimidine-2,4,6-trione

: 159042-29-2
1-(3,5-di-O-acetyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-5-benzyluracil

Guidance literature:: Multi-step reaction with 5 steps

2: (NH₄)2SO₄ / 2 h / Heating

3: 55 percent / CH₂Cl₂ / 120 h / Ambient temperature

4: NH₃, MeOH / 48 h / Ambient temperature

5: pyridine

With pyridine; methanol; ammonium sulfate; ammonia; In dichloromethane;
DOI:10.1080/15257779408013228

Reference yield:

: 56632-81-6
1,3-di-O-acetyl-5-O-benzoyl-2-deoxy-2-fluoro-D-arabinofuranosyl bromide

: 159042-29-2
1-(3,5-di-O-acetyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-5-benzyluracil

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / CH₂Cl₂ / 120 h / Ambient temperature

2: NH₃, MeOH / 48 h / Ambient temperature

3: pyridine

With pyridine; methanol; ammonia; In dichloromethane;
DOI:10.1080/15257779408013228