dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside

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Chemical Name:dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:1080017-62-4
Molecular Formula:C₂₅H₃₉N₃O₇Si
Molecular Weight:521.686
Hs Code.:

Synonyms:dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside

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Technology Process of dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 2 articles about dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: C₂₅H₃₇N₃O₇Si

: 1080017-62-4
dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With triethylsilane; phenylborondichloride; In dichloromethane; at -75 ℃; for 1h; Molecular sieve;

Reference yield: 94.0%

: 1129412-85-6
dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 1080017-62-4
dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With triethylsilane; 4 A molecular sieve; phenylborondichloride; In dichloromethane; at -75 ℃; for 1h;
DOI:10.1002/chem.200701165

Reference yield: 94.0%

: 1080017-62-4
dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside

: 4,6-O-benzylidene-2-deoxy-2-(9-fluorenylmethoxycarbonylamino)-3-O-levulinoyl-D-glucopyranosyl trichloroacetimidate

: dimethylthexylsilyl 6-O-[4,6-O-benzylidene-2-deoxy-2-(9-fluorenylmethoxycarbonyl amino)-3-O-leyulinoyl-β-D-glucopyranosyl]-3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside; 4,6-O-benzylidene-2-deoxy-2-(9-fluorenylmethoxycarbonylamino)-3-O-levulinoyl-D-glucopyranosyl trichloroacetimidate; In dichloromethane; at 20 ℃; for 1h; Molecular sieve;

With trifluorormethanesulfonic acid; In dichloromethane; at -50 - -20 ℃; for 1.25h;