dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside
CAS No.:1129412-85-6
Molecular Formula:C₂₅H₃₇N₃O₇Si
Molecular Weight:519.67
Hs Code.:

Synonyms:dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

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Technology Process of dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

There total 1 articles about dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 157488-91-0
thexyldimethylsilyl 2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 2937-50-0
Allyl chloroformate

: 1129412-85-6
dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1002/chem.200701165

Reference yield: 94.0%

: 1129412-85-6
dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 1080017-62-4
dimethylthexylsilyl 3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With triethylsilane; 4 A molecular sieve; phenylborondichloride; In dichloromethane; at -75 ℃; for 1h;
DOI:10.1002/chem.200701165