N,N'-(3,7,13,17-tetraoxo-4,8,12,16-tetraazanonadecane-1,19-diyl)bis(4-hydroxybenzamide)

Base Information

Chemical Name:N,N'-(3,7,13,17-tetraoxo-4,8,12,16-tetraazanonadecane-1,19-diyl)bis(4-hydroxybenzamide)
CAS No.:1227367-60-3
Molecular Formula:C₂₉H₃₈N₆O₈
Molecular Weight:598.656
Hs Code.:

Synonyms:N,N'-(3,7,13,17-tetraoxo-4,8,12,16-tetraazanonadecane-1,19-diyl)bis(4-hydroxybenzamide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-(3,7,13,17-tetraoxo-4,8,12,16-tetraazanonadecane-1,19-diyl)bis(4-hydroxybenzamide)

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Technology Process of N,N'-(3,7,13,17-tetraoxo-4,8,12,16-tetraazanonadecane-1,19-diyl)bis(4-hydroxybenzamide)

There total 5 articles about N,N'-(3,7,13,17-tetraoxo-4,8,12,16-tetraazanonadecane-1,19-diyl)bis(4-hydroxybenzamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1227185-32-1
C₁₅H₃₀N₆O₄

: 99-96-7
4-hydroxy-benzoic acid

: 1227367-60-3
N,N'-(3,7,13,17-tetraoxo-4,8,12,16-tetraazanonadecane-1,19-diyl)bis(4-hydroxybenzamide)

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 20h;
DOI:10.1002/anie.200906114

Reference yield: 61.0%

: 773838-08-7
3-(4-hydroxybenzamido)propanoic acid

: C₉H₂₀N₄O₂*2ClH

: 1227367-60-3
N,N'-(3,7,13,17-tetraoxo-4,8,12,16-tetraazanonadecane-1,19-diyl)bis(4-hydroxybenzamide)

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 21h;

Reference yield: 61.0%

: 1227185-30-9
tert-butyl 3,3'-(propane-1,3-diylbis(azanediyl))bis(3-oxopropane-3,1-diyl)dicarbamate

: 773838-08-7
3-(4-hydroxybenzamido)propanoic acid

: 1227367-60-3
N,N'-(3,7,13,17-tetraoxo-4,8,12,16-tetraazanonadecane-1,19-diyl)bis(4-hydroxybenzamide)

Guidance literature:: tert-butyl 3,3'-(propane-1,3-diylbis(azanediyl))bis(3-oxopropane-3,1-diyl)dicarbamate; With hydrogenchloride; In methanol; at 50 ℃; for 2.25h; Inert atmosphere; Sonication;

3-(4-hydroxybenzamido)propanoic acid; With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 21h; Inert atmosphere;
DOI:10.1002/ejoc.201001695