1,2,5-trimethyl-4-aminopiperidine

Base Information

Chemical Name:1,2,5-trimethyl-4-aminopiperidine
CAS No.:136038-93-2
Molecular Formula:C₁₇H₂₄Cl₂N₂O₂
Molecular Weight:359.296
Hs Code.:

1,2,5-trimethyl-4-<N-(3,4-dichlorophenyl)-N-ethoxycarbonyl>aminopiperidine

Synonyms:1,2,5-trimethyl-4-aminopiperidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2,5-trimethyl-4-aminopiperidine

Chemical Property:

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Technology Process of 1,2,5-trimethyl-4-aminopiperidine

There total 3 articles about 1,2,5-trimethyl-4-aminopiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 541-41-3
chloroformic acid ethyl ester

: 136038-85-2
1,2,5-trimethyl-4-N-(3,4-dichlorophenyl)aminopiperidine

: 136038-93-2
1,2,5-trimethyl-4-aminopiperidine

Guidance literature:: With triethylamine; In diethyl ether; at 20 ℃; for 12h;
DOI:10.1007/BF00772136

Reference yield:

: 136038-82-9
N-(1,2,5-trimethyl-4-piperidylidene)-3,4-dichloroaniline

: 136038-93-2
1,2,5-trimethyl-4-aminopiperidine

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / NaBH₄ / propan-2-ol / 3 h / 60 °C

2: 58 percent / Et₃N / diethyl ether / 12 h / 20 °C

With sodium tetrahydroborate; triethylamine; In diethyl ether; isopropyl alcohol;
DOI:10.1007/BF00772136

Reference yield:

: 95-76-1
m,p-dichloroaniline

: 136038-93-2
1,2,5-trimethyl-4-aminopiperidine

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / acetic acid / toluene / 8 h / Heating

2: 46 percent / NaBH₄ / propan-2-ol / 3 h / 60 °C

3: 58 percent / Et₃N / diethyl ether / 12 h / 20 °C

With sodium tetrahydroborate; acetic acid; triethylamine; In diethyl ether; isopropyl alcohol; toluene;
DOI:10.1007/BF00772136