(Z)-1-methyl-3-(2-phenyl-2-m-tolylvinyl)benzene

Base Information

Chemical Name:(Z)-1-methyl-3-(2-phenyl-2-m-tolylvinyl)benzene
CAS No.:1059620-01-7
Molecular Formula:C₂₂H₂₀
Molecular Weight:284.401
Hs Code.:

Synonyms:(Z)-1-methyl-3-(2-phenyl-2-m-tolylvinyl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1-methyl-3-(2-phenyl-2-m-tolylvinyl)benzene

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Technology Process of (Z)-1-methyl-3-(2-phenyl-2-m-tolylvinyl)benzene

There total 5 articles about (Z)-1-methyl-3-(2-phenyl-2-m-tolylvinyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 2765-16-4
bis(3-methylphenyl)acetylene

: 100-58-3
phenylmagnesium bromide

: 1059620-01-7
(Z)-1-methyl-3-(2-phenyl-2-m-tolylvinyl)benzene

Guidance literature:: bis(3-methylphenyl)acetylene; phenylmagnesium bromide; With nickel(II) chloride hexahydrate; In tetrahydrofuran; toluene; at 20 ℃; for 1h; Inert atmosphere; Schlenk technique;

With water; In tetrahydrofuran; toluene; stereoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1039/c3cc45202f

Reference yield: 72.0%

: 2765-16-4
bis(3-methylphenyl)acetylene

: 98-80-6
phenylboronic acid

: 1059620-01-7
(Z)-1-methyl-3-(2-phenyl-2-m-tolylvinyl)benzene

Guidance literature:: acetylacetonatodicarbonylrhodium(l); In water; toluene; at 110 ℃; for 12h;
DOI:10.1016/j.tetlet.2008.05.140

Reference yield: 58.0%

: 2765-16-4
bis(3-methylphenyl)acetylene

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 1059620-01-7
(Z)-1-methyl-3-(2-phenyl-2-m-tolylvinyl)benzene

Guidance literature:: With palladium diacetate; silver carbonate; 2-hydroxyl-1,10-phenanthroline; at 120 ℃; for 15h; Sealed tube;
DOI:10.1002/anie.201808866