2,3,4-tri-O-benzyl-L-arabino-pentodialdose 1,1-di(n-propyl)dithioacetal

Base Information

Chemical Name:2,3,4-tri-O-benzyl-L-arabino-pentodialdose 1,1-di(n-propyl)dithioacetal
CAS No.:153322-92-0
Molecular Formula:C₃₂H₄₀O₄S₂
Molecular Weight:552.799
Hs Code.:

Synonyms:2,3,4-tri-O-benzyl-L-arabino-pentodialdose 1,1-di(n-propyl)dithioacetal

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Chemical Property of 2,3,4-tri-O-benzyl-L-arabino-pentodialdose 1,1-di(n-propyl)dithioacetal

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Technology Process of 2,3,4-tri-O-benzyl-L-arabino-pentodialdose 1,1-di(n-propyl)dithioacetal

There total 1 articles about 2,3,4-tri-O-benzyl-L-arabino-pentodialdose 1,1-di(n-propyl)dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 153226-04-1
2,3,4-tri-O-benzyl-D-galactose 1,1-di(n-propyl)dithioacetal

: 153322-92-0
2,3,4-tri-O-benzyl-L-arabino-pentodialdose 1,1-di(n-propyl)dithioacetal

Guidance literature:: With lead(IV) acetate; In benzene; for 2h; Ambient temperature;
DOI:10.1016/S0957-4166(00)80076-2

Reference yield:

: 1779-49-3
Methyltriphenylphosphonium bromide

: 153322-92-0
2,3,4-tri-O-benzyl-L-arabino-pentodialdose 1,1-di(n-propyl)dithioacetal

: 343934-78-1
(2R,3S,4S)-2,3,4-tribenzyloxy-hex-5-ene-1-al di-n-propyl dithioacetal

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In hexane; toluene; at 0 ℃; for 1h;

2,3,4-tri-O-benzyl-L-arabino-pentodialdose 1,1-di(n-propyl)dithioacetal; In toluene; at 0 ℃; for 2h;
DOI:10.1016/S0957-4166(01)00050-7

Reference yield:

: 153322-92-0
2,3,4-tri-O-benzyl-L-arabino-pentodialdose 1,1-di(n-propyl)dithioacetal

: 343934-79-2
N-(4-Bromo-phenyl)-N'-[(2S,3S,4S)-2,3,4-tris-benzyloxy-hex-5-en-(E)-ylidene]-hydrazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: BuLi / toluene; hexane / 1 h / 0 °C

1.2: 250 mg / toluene / 2 h / 0 °C

2.1: HgCl₂; CdCO₃ / acetone; H₂O / 24 h

3.1: 225 mg / aq. NaHCO₃ / CH₂Cl₂

With n-butyllithium; cadmium(II) carbonate; sodium hydrogencarbonate; mercury dichloride; In hexane; dichloromethane; water; acetone; toluene; 1.2: Wittig reaction;
DOI:10.1016/S0957-4166(01)00050-7