(2R)-2-Azido-2-<(3-(benzyloxy)-4-methoxy)phenyl>acetic acid ethyl ester

Base Information

Chemical Name:(2R)-2-Azido-2-<(3-(benzyloxy)-4-methoxy)phenyl>acetic acid ethyl ester
CAS No.:169176-59-4
Molecular Formula:C₁₈H₁₉N₃O₄
Molecular Weight:341.367
Hs Code.:

Synonyms:(2R)-2-Azido-2-<(3-(benzyloxy)-4-methoxy)phenyl>acetic acid ethyl ester

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Chemical Property of (2R)-2-Azido-2-<(3-(benzyloxy)-4-methoxy)phenyl>acetic acid ethyl ester

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Technology Process of (2R)-2-Azido-2-<(3-(benzyloxy)-4-methoxy)phenyl>acetic acid ethyl ester

There total 2 articles about (2R)-2-Azido-2-<(3-(benzyloxy)-4-methoxy)phenyl>acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 64-17-5
ethanol

: 159579-64-3
(2R)-2-Azido-2-<(3-(benzyloxy)-4-methoxy)phenyl>acetic acid

: 169176-59-4
(2R)-2-Azido-2-<(3-(benzyloxy)-4-methoxy)phenyl>acetic acid ethyl ester

Guidance literature:: With toluene-4-sulfonic acid; for 8h; Heating;
DOI:10.1021/jo00127a020

Reference yield:

: 64-17-5
ethanol

: (R)-3-[(R)-2-Azido-2-(3-benzyloxy-4-methoxy-phenyl)-acetyl]-4-benzyl-oxazolidin-2-one

: 169176-59-4
(2R)-2-Azido-2-<(3-(benzyloxy)-4-methoxy)phenyl>acetic acid ethyl ester

: 3-Benzyloxy-4-methoxy-benzoic acid ethyl ester

Guidance literature:: With lithium hydroxide; dihydrogen peroxide; toluene-4-sulfonic acid; Multistep reaction; 1) THF, H₂O, 0 deg C, 0.5 - 1 h, 2) reflux, overnight;
DOI:10.1021/jo961637x

Reference yield: 99.0%

: 169176-59-4
(2R)-2-Azido-2-<(3-(benzyloxy)-4-methoxy)phenyl>acetic acid ethyl ester

: 169176-60-7
D-<(3-Hydroxy-4-methoxy)phenyl>glycine ethyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; for 24h; under 735.5 Torr; Ambient temperature;
DOI:10.1021/jo00127a020