2-<<3-nitro-2-<<5-<(tert-butyldimethylsilyl)oxy>pentyl>thio>phenyl>methylene>-3-oxobutanoic acid, 2-(trimethylsilyl)ethyl ester

Base Information

Chemical Name:2-<<3-nitro-2-<<5-<(tert-butyldimethylsilyl)oxy>pentyl>thio>phenyl>methylene>-3-oxobutanoic acid, 2-(trimethylsilyl)ethyl ester
CAS No.:145457-73-4
Molecular Formula:C₂₇H₄₅NO₆SSi₂
Molecular Weight:567.894
Hs Code.:

Synonyms:2-<<3-nitro-2-<<5-<(tert-butyldimethylsilyl)oxy>pentyl>thio>phenyl>methylene>-3-oxobutanoic acid, 2-(trimethylsilyl)ethyl ester

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Chemical Property of 2-<<3-nitro-2-<<5-<(tert-butyldimethylsilyl)oxy>pentyl>thio>phenyl>methylene>-3-oxobutanoic acid, 2-(trimethylsilyl)ethyl ester

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Technology Process of 2-<<3-nitro-2-<<5-<(tert-butyldimethylsilyl)oxy>pentyl>thio>phenyl>methylene>-3-oxobutanoic acid, 2-(trimethylsilyl)ethyl ester

There total 2 articles about 2-<<3-nitro-2-<<5-<(tert-butyldimethylsilyl)oxy>pentyl>thio>phenyl>methylene>-3-oxobutanoic acid, 2-(trimethylsilyl)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 17165-45-6
2-(trimethylsilyl)ethyl acetoacetate

: 3-nitro-2-<5-<(tert-butyldimethylsilyl)oxy>pentyl>thiobenzaldehyde

: 145457-73-4
2-<<3-nitro-2-<<5-<(tert-butyldimethylsilyl)oxy>pentyl>thio>phenyl>methylene>-3-oxobutanoic acid, 2-(trimethylsilyl)ethyl ester

Guidance literature:: With piperidine; acetic acid; In benzene; for 1h; Heating;
DOI:10.1021/jm00001a017

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 145457-73-4
2-<<3-nitro-2-<<5-<(tert-butyldimethylsilyl)oxy>pentyl>thio>phenyl>methylene>-3-oxobutanoic acid, 2-(trimethylsilyl)ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate / toluene / 90 °C

2: 82 percent / acetic acid, piperidine / benzene / 1 h / Heating

With piperidine; sodium acetate; acetic acid; In toluene; benzene;
DOI:10.1021/jm00001a017