C₂₁H₂₂FIO₄

Base Information

Chemical Name:C₂₁H₂₂FIO₄
CAS No.:1142228-96-3
Molecular Formula:C₂₁H₂₂FIO₄
Molecular Weight:484.306
Hs Code.:

C<sub>21</sub>H<sub>22</sub>FIO<sub>4</sub>

Synonyms:C₂₁H₂₂FIO₄

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Chemical Property of C₂₁H₂₂FIO₄

Chemical Property:

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Technology Process of C₂₁H₂₂FIO₄

There total 5 articles about C₂₁H₂₂FIO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1142227-22-2
2'-fluoro-2-(1-hydroxy-2,2-dimethyl-but-3-enyl)-5'-methoxy-biphenyl-4-carboxylic acid methyl ester

: 1142228-96-3
C₂₁H₂₂FIO₄

Guidance literature:: With iodine; sodium hydrogencarbonate; In acetonitrile; at 20 ℃; for 16h;

Reference yield:

: 24589-99-9
methyl 3-formyl-4-hydroxybenzoate

: 1142228-96-3
C₂₁H₂₂FIO₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; triethylamine / dichloromethane / 0.33 h / 20 °C

1.2: 0.5 h / 20 °C

2.1: potassium phosphate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 6 h / 90 °C / Inert atmosphere

3.1: indium; sodium iodide / N,N-dimethyl-formamide / 2 h / 20 °C

4.1: iodine; sodium hydrogencarbonate / acetonitrile / 16 h / 20 °C

With dmap; indium; potassium phosphate; iodine; sodium hydrogencarbonate; triethylamine; sodium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 952041-75-7
methyl 3-formyl-4-(((trifluoromethyl)sulfonyl)oxy)benzoate

: 1142228-96-3
C₂₁H₂₂FIO₄

Guidance literature:: Multi-step reaction with 3 steps

1: potassium phosphate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 6 h / 90 °C / Inert atmosphere

2: indium; sodium iodide / N,N-dimethyl-formamide / 2 h / 20 °C

3: iodine; sodium hydrogencarbonate / acetonitrile / 16 h / 20 °C

With indium; potassium phosphate; iodine; sodium hydrogencarbonate; sodium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; acetonitrile;