C₆₄H₈₂O₁₆

Base Information

Chemical Name:C₆₄H₈₂O₁₆
CAS No.:318262-32-7
Molecular Formula:C₆₄H₈₂O₁₆
Molecular Weight:1107.35
Hs Code.:

C<sub>64</sub>H<sub>82</sub>O<sub>16</sub>

Synonyms:C₆₄H₈₂O₁₆

Suppliers and Price of C₆₄H₈₂O₁₆

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₄H₈₂O₁₆

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₄H₈₂O₁₆

There total 17 articles about C₆₄H₈₂O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 318262-31-6
C₆₇H₉₀O₁₆Si

: 318262-32-7
C₆₄H₈₂O₁₆

Guidance literature:: With tetrabutyl ammonium fluoride; water; In tetrahydrofuran; at 20 ℃; for 0.00833333h;
DOI:10.1021/ja002129e

Reference yield:

: 6307-83-1
3-bromo-5-nitro-benzoic acid

: 318262-32-7
C₆₄H₈₂O₁₆

Guidance literature:: Multi-step reaction with 12 steps

1: 85 percent / BH₃*THF / tetrahydrofuran / 16 h / 20 °C

2: 92 percent / PCl₅ / CHCl₃ / 12 h / Heating

3: 84 percent / Bu₄NI; aq. NaOH / CH₂Cl₂ / 24 h / 20 °C

4: 90 percent / hydrazine hydrate; graphite / ethanol / 11 h / Heating

5: 98 percent / BF₃*OEt₂; t-butyl nitrite / tetrahydrofuran / -15 °C

6: 93 percent / K₂CO₃ / CH₂Cl₂ / 1 h / 0 °C

7: 80 percent / CuI; PPh₃; Et₃N / Pd₂(dba)3 / 41 h / 70 °C

8: 80 percent / CH₃I / 12 h / 110 °C

9: 84 percent / CuI; PPh₃; NEt₃ / Pd₂(dba)3 / 70 °C

10: 98 percent / TBAF; H₂O / tetrahydrofuran / 0.01 h / 20 °C

11: 83 percent / CuI; PPh₃; NEt₃ / Pd₂(dba)3 / 70 °C

12: 98 percent / TBAF; H₂O / tetrahydrofuran / 0.01 h / 20 °C

With sodium hydroxide; copper(l) iodide; tert.-butylnitrite; borane-THF; phosphorus pentachloride; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; water; tetra-(n-butyl)ammonium iodide; potassium carbonate; pyrographite; hydrazine hydrate; triethylamine; triphenylphosphine; methyl iodide; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; ethanol; dichloromethane; chloroform; 7: Sonogashira coupling;
DOI:10.1021/ja002129e

Reference yield:

: 318261-49-3
1-bromo-3-(chloromethyl)-5-nitrobenzene

: 318262-32-7
C₆₄H₈₂O₁₆

Guidance literature:: Multi-step reaction with 10 steps

1: 84 percent / Bu₄NI; aq. NaOH / CH₂Cl₂ / 24 h / 20 °C

2: 90 percent / hydrazine hydrate; graphite / ethanol / 11 h / Heating

3: 98 percent / BF₃*OEt₂; t-butyl nitrite / tetrahydrofuran / -15 °C

4: 93 percent / K₂CO₃ / CH₂Cl₂ / 1 h / 0 °C

5: 80 percent / CuI; PPh₃; Et₃N / Pd₂(dba)3 / 41 h / 70 °C

6: 80 percent / CH₃I / 12 h / 110 °C

7: 84 percent / CuI; PPh₃; NEt₃ / Pd₂(dba)3 / 70 °C

8: 98 percent / TBAF; H₂O / tetrahydrofuran / 0.01 h / 20 °C

9: 83 percent / CuI; PPh₃; NEt₃ / Pd₂(dba)3 / 70 °C

10: 98 percent / TBAF; H₂O / tetrahydrofuran / 0.01 h / 20 °C

With sodium hydroxide; copper(l) iodide; tert.-butylnitrite; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; water; tetra-(n-butyl)ammonium iodide; potassium carbonate; pyrographite; hydrazine hydrate; triethylamine; triphenylphosphine; methyl iodide; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; ethanol; dichloromethane; 5: Sonogashira coupling;
DOI:10.1021/ja002129e