2,6-difluoro-N-hydroxybenzamide

Base Information

Chemical Name:2,6-difluoro-N-hydroxybenzamide
CAS No.:125309-34-4
Molecular Formula:C₇H₅F₂NO₂
Molecular Weight:173.119
Hs Code.:2924297099
Mol file:125309-34-4.mol

Synonyms:2,6-difluoro-N-hydroxybenzamide

Suppliers and Price of 2,6-difluoro-N-hydroxybenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Atlantic Research Chemicals
2,6-Difluoro-N-hydroxybenzamide 95%
1gm:
$ 258.02

Total 2 raw suppliers

Chemical Property of 2,6-difluoro-N-hydroxybenzamide

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

2,6-Difluoro-N-hydroxybenzamide 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,6-difluoro-N-hydroxybenzamide

There total 3 articles about 2,6-difluoro-N-hydroxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 13671-00-6
methyl 2,6-difluorobenzoate

: 125309-34-4
2,6-difluoro-N-hydroxybenzamide

Guidance literature:: With hydroxylamine hydrochloride; potassium hydroxide; In methanol; water; at 0 - 25 ℃; for 17h;
DOI:10.1021/acs.oprd.5b00389

Reference yield: 54.0%

: 13671-00-6
methyl 2,6-difluorobenzoate

: 125309-34-4
2,6-difluoro-N-hydroxybenzamide

: 385-00-2
2,6-difluorobenzoic acid

Guidance literature:: With hydroxylamine; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; water; at 20 ℃; for 2h;
DOI:10.1016/j.tetlet.2016.04.003

Reference yield:

: 385-00-2
2,6-difluorobenzoic acid

: 125309-34-4
2,6-difluoro-N-hydroxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 40 h / Heating

2: hydroxylamine hydrochloride; potassium hydroxide / water; methanol / 17 h / 0 - 25 °C

With sulfuric acid; hydroxylamine hydrochloride; potassium hydroxide; In methanol; water;
DOI:10.1021/acs.oprd.5b00389