methyl 3-[6-[(1E)-3-tert-butoxy-3-oxo-prop-1-en-1-yl]-4-oxo-4H-quinazolin-3-yl]-4-methylbenzoate

Base Information

Chemical Name:methyl 3-[6-[(1E)-3-tert-butoxy-3-oxo-prop-1-en-1-yl]-4-oxo-4H-quinazolin-3-yl]-4-methylbenzoate
CAS No.:907574-57-6
Molecular Formula:C₂₄H₂₄N₂O₅
Molecular Weight:420.465
Hs Code.:

Synonyms:methyl 3-[6-[(1E)-3-tert-butoxy-3-oxo-prop-1-en-1-yl]-4-oxo-4H-quinazolin-3-yl]-4-methylbenzoate

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Chemical Property of methyl 3-[6-[(1E)-3-tert-butoxy-3-oxo-prop-1-en-1-yl]-4-oxo-4H-quinazolin-3-yl]-4-methylbenzoate

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Technology Process of methyl 3-[6-[(1E)-3-tert-butoxy-3-oxo-prop-1-en-1-yl]-4-oxo-4H-quinazolin-3-yl]-4-methylbenzoate

There total 1 articles about methyl 3-[6-[(1E)-3-tert-butoxy-3-oxo-prop-1-en-1-yl]-4-oxo-4H-quinazolin-3-yl]-4-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 851847-27-3
methyl 3-(6-bromo-4-oxo-4H-quinazolin-3-yl)-4-methyl-benzoate

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 907574-57-6
methyl 3-[6-[(1E)-3-tert-butoxy-3-oxo-prop-1-en-1-yl]-4-oxo-4H-quinazolin-3-yl]-4-methylbenzoate

Guidance literature:: With triethylamine; 1,2,3,4,5-pentaphenyl-1-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 20 - 100 ℃; for 77h;

Reference yield:

: 907574-57-6
methyl 3-[6-[(1E)-3-tert-butoxy-3-oxo-prop-1-en-1-yl]-4-oxo-4H-quinazolin-3-yl]-4-methylbenzoate

: 907574-58-7
methyl 3-(6-formyl-4-oxoquinazolin-3(4H)-yl)-4-methylbenzoate

Guidance literature:: With sodium periodate; osmium(VIII) oxide; In tetrahydrofuran; water; tert-butyl alcohol; at 20 ℃; for 72h;

Reference yield:

: 907574-57-6
methyl 3-[6-[(1E)-3-tert-butoxy-3-oxo-prop-1-en-1-yl]-4-oxo-4H-quinazolin-3-yl]-4-methylbenzoate

: 926318-41-4
3-[6-[(E)-2-carboxyvinyl]-4-oxo-4H-quinazolin-3-yl]-4-methyl-benzoic acid

Guidance literature:: methyl 3-[6-[(1E)-3-tert-butoxy-3-oxo-prop-1-en-1-yl]-4-oxo-4H-quinazolin-3-yl]-4-methylbenzoate; With methanol; sodium hydroxide; water; at 17 - 65 ℃;

With hydrogenchloride; water; In methanol; pH=~ 3;