methyl 2-[3-(tert-butylamino)-2-phenylimidazo[1,2-a]pyridin-8-yl]-1-(3-methoxypropyl)-1H-benzo[d]imidazole-5-carboxylate

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Chemical Name:methyl 2-[3-(tert-butylamino)-2-phenylimidazo[1,2-a]pyridin-8-yl]-1-(3-methoxypropyl)-1H-benzo[d]imidazole-5-carboxylate
CAS No.:1430101-54-4
Molecular Formula:C₃₀H₃₃N₅O₃
Molecular Weight:511.624
Hs Code.:

Synonyms:methyl 2-[3-(tert-butylamino)-2-phenylimidazo[1,2-a]pyridin-8-yl]-1-(3-methoxypropyl)-1H-benzo[d]imidazole-5-carboxylate

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Chemical Property of methyl 2-[3-(tert-butylamino)-2-phenylimidazo[1,2-a]pyridin-8-yl]-1-(3-methoxypropyl)-1H-benzo[d]imidazole-5-carboxylate

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Technology Process of methyl 2-[3-(tert-butylamino)-2-phenylimidazo[1,2-a]pyridin-8-yl]-1-(3-methoxypropyl)-1H-benzo[d]imidazole-5-carboxylate

There total 2 articles about methyl 2-[3-(tert-butylamino)-2-phenylimidazo[1,2-a]pyridin-8-yl]-1-(3-methoxypropyl)-1H-benzo[d]imidazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 1430101-82-8
methyl 2-(2-amino-3-pyridyl)-1-(3-methoxypropyl)-1H-benzo[d]imidazole-5-carboxylate

: 100-52-7
benzaldehyde

: 1430101-54-4
methyl 2-[3-(tert-butylamino)-2-phenylimidazo[1,2-a]pyridin-8-yl]-1-(3-methoxypropyl)-1H-benzo[d]imidazole-5-carboxylate

Guidance literature:: With scandium tris(trifluoromethanesulfonate); In neat (no solvent); at 135 ℃; Microwave irradiation; Inert atmosphere; Green chemistry;
DOI:10.1021/co400010y

Reference yield:

: 1430101-78-2
methyl 3-[(2-amino-3-pyridyl)carbonyl]amino-4-[(3-methoxypropyl)amino]benzoate

: 1430101-54-4
methyl 2-[3-(tert-butylamino)-2-phenylimidazo[1,2-a]pyridin-8-yl]-1-(3-methoxypropyl)-1H-benzo[d]imidazole-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid; magnesium sulfate / 1,2-dichloro-ethane / 0.17 h / 130 °C / Microwave irradiation; Inert atmosphere

2: scandium tris(trifluoromethanesulfonate) / neat (no solvent) / 135 °C / Microwave irradiation; Inert atmosphere; Green chemistry

With magnesium sulfate; trifluoroacetic acid; scandium tris(trifluoromethanesulfonate); In 1,2-dichloro-ethane;
DOI:10.1021/co400010y