C₃₁H₃₃FN₂O₄

Base Information

Chemical Name:C₃₁H₃₃FN₂O₄
CAS No.:1418718-38-3
Molecular Formula:C₃₁H₃₃FN₂O₄
Molecular Weight:516.612
Hs Code.:

C<sub>31</sub>H<sub>33</sub>FN<sub>2</sub>O<sub>4</sub>

Synonyms:C₃₁H₃₃FN₂O₄

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Chemical Property of C₃₁H₃₃FN₂O₄

Chemical Property:

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Technology Process of C₃₁H₃₃FN₂O₄

There total 15 articles about C₃₁H₃₃FN₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1418718-29-2
methyl 2-(tert-butoxy)-2-(4-(chroman-6-yl)-6-methyl-1H-pyrrolo[2,3-b]pyridin-5-yl)acetate

: 459-46-1
4-Fluorobenzyl bromide

: 1418718-38-3
C₃₁H₃₃FN₂O₄

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 1.33333h; under 760.051 Torr;

Reference yield:

: 493-08-3
chromane

: 1418718-38-3
C₃₁H₃₃FN₂O₄

Guidance literature:: Multi-step reaction with 14 steps

1.1: iodine; silver nitrate / methanol / 1 h / 760.05 Torr

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -78 °C / 760.05 Torr

2.2: 0.17 h / 20 °C / 760.05 Torr

3.1: piperidine; acetic acid / benzene / 760.05 Torr / Reflux

4.1: 4-methyl-morpholine / isopropyl alcohol / 90 °C / 760.05 Torr

5.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C / 760.05 Torr

6.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 0.08 h / 0 °C / 760.05 Torr

7.1: pyridinium chlorochromate / dichloromethane / 20 °C / 760.05 Torr

8.1: caesium carbonate / methanol; hexane / 60 °C / 760.05 Torr

9.1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / 760.05 Torr / Cooling with ice

10.1: pyridinium chlorochromate / dichloromethane / 1.5 h / 20 °C / 760.05 Torr

11.1: zinc(II) iodide / dichloromethane / 0.17 h / 760.05 Torr / Cooling with ice

12.1: sulfuric acid / 0 - 80 °C / 760.05 Torr

13.1: perchloric acid / 20 °C / 760.05 Torr

14.1: caesium carbonate / N,N-dimethyl-formamide / 1.33 h / 80 °C / 760.05 Torr

With piperidine; 4-methyl-morpholine; lithium aluminium tetrahydride; n-butyllithium; perchloric acid; sulfuric acid; iodine; caesium carbonate; silver nitrate; acetic acid; sodium bis(2-methoxyethoxy)aluminium dihydride; pyridinium chlorochromate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; zinc(II) iodide; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol; toluene; benzene;

Reference yield:

: 491-37-2
2,3-dihydro-4H-1-benzopyran-4-one

: 1418718-38-3
C₃₁H₃₃FN₂O₄

Guidance literature:: Multi-step reaction with 15 steps

1.1: acetic acid; zinc / 100 °C / 760.05 Torr

2.1: iodine; silver nitrate / methanol / 1 h / 760.05 Torr

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -78 °C / 760.05 Torr

3.2: 0.17 h / 20 °C / 760.05 Torr

4.1: piperidine; acetic acid / benzene / 760.05 Torr / Reflux

5.1: 4-methyl-morpholine / isopropyl alcohol / 90 °C / 760.05 Torr

6.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C / 760.05 Torr

7.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 0.08 h / 0 °C / 760.05 Torr

8.1: pyridinium chlorochromate / dichloromethane / 20 °C / 760.05 Torr

9.1: caesium carbonate / methanol; hexane / 60 °C / 760.05 Torr

10.1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / 760.05 Torr / Cooling with ice

11.1: pyridinium chlorochromate / dichloromethane / 1.5 h / 20 °C / 760.05 Torr

12.1: zinc(II) iodide / dichloromethane / 0.17 h / 760.05 Torr / Cooling with ice

13.1: sulfuric acid / 0 - 80 °C / 760.05 Torr

14.1: perchloric acid / 20 °C / 760.05 Torr

15.1: caesium carbonate / N,N-dimethyl-formamide / 1.33 h / 80 °C / 760.05 Torr

With piperidine; 4-methyl-morpholine; lithium aluminium tetrahydride; n-butyllithium; perchloric acid; sulfuric acid; iodine; caesium carbonate; silver nitrate; acetic acid; sodium bis(2-methoxyethoxy)aluminium dihydride; pyridinium chlorochromate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; zinc(II) iodide; zinc; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol; toluene; benzene;