7-chloro-5-phenyl-3-methyl-2,2,3,3'-tetradeuterio-1,3-dihydro-2H-1,4-benzodiazepine

Base Information

Chemical Name:7-chloro-5-phenyl-3-methyl-2,2,3,3'-tetradeuterio-1,3-dihydro-2H-1,4-benzodiazepine
CAS No.:88369-22-6
Molecular Formula:C₁₆H₁₅ClN₂
Molecular Weight:274.73
Hs Code.:

Synonyms:7-chloro-5-phenyl-3-methyl-2,2,3,3'-tetradeuterio-1,3-dihydro-2H-1,4-benzodiazepine

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Chemical Property of 7-chloro-5-phenyl-3-methyl-2,2,3,3'-tetradeuterio-1,3-dihydro-2H-1,4-benzodiazepine

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Technology Process of 7-chloro-5-phenyl-3-methyl-2,2,3,3'-tetradeuterio-1,3-dihydro-2H-1,4-benzodiazepine

There total 4 articles about 7-chloro-5-phenyl-3-methyl-2,2,3,3'-tetradeuterio-1,3-dihydro-2H-1,4-benzodiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 88369-21-5
C₂₃H₁₈⁽²⁾HClN₂O₄S

: 88369-22-6
7-chloro-5-phenyl-3-methyl-2,2,3,3'-tetradeuterio-1,3-dihydro-2H-1,4-benzodiazepine

Guidance literature:: With lithium aluminium deuteride; In tetrahydrofuran; for 16h; Ambient temperature;
DOI:10.1002/jhet.5570200534

Reference yield:

: 88369-19-1
7-chloro-5-phenyl-3-hydroxymethyl-3-deuterio-1,3-dihydro-2H-1,4-benzodiazepin-2-one

: 88369-22-6
7-chloro-5-phenyl-3-methyl-2,2,3,3'-tetradeuterio-1,3-dihydro-2H-1,4-benzodiazepine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 2 h / Ambient temperature

2: 69 percent / LiAlD₄ / tetrahydrofuran / 16 h / Ambient temperature

With pyridine; lithium aluminium deuteride; In tetrahydrofuran;
DOI:10.1002/jhet.5570200534

Reference yield:

: 88369-18-0
7-chloro-3-(ethoxycarbonyl)-5-phenyl-<3-2H₁>-1,3-dihydro-2H-1,4-benzodiazepin-2-one

: 88369-22-6
7-chloro-5-phenyl-3-methyl-2,2,3,3'-tetradeuterio-1,3-dihydro-2H-1,4-benzodiazepine

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / sodium diethyldihydroaluminate / toluene; tetrahydrofuran / 0.5 h / Ambient temperature

2: pyridine / 2 h / Ambient temperature

3: 69 percent / LiAlD₄ / tetrahydrofuran / 16 h / Ambient temperature

With pyridine; lithium aluminium deuteride; sodium aluminum diethyl dihydride; In tetrahydrofuran; toluene;
DOI:10.1002/jhet.5570200534