1-Ethyl-2-{(1E,3E,5E)-7-[1-ethyl-3,3-dimethyl-1,3-dihydro-indol-(2Z)-ylidene]-hepta-1,3,5-trienyl}-3,3-dimethyl-5-[4-((1Z,4Z,9Z,15Z)-10,15,20-triphenyl-porphyrin-5-yl)-phenylcarbamoyl]-3H-indolium; iodide

Base Information

Chemical Name:1-Ethyl-2-{(1E,3E,5E)-7-[1-ethyl-3,3-dimethyl-1,3-dihydro-indol-(2Z)-ylidene]-hepta-1,3,5-trienyl}-3,3-dimethyl-5-[4-((1Z,4Z,9Z,15Z)-10,15,20-triphenyl-porphyrin-5-yl)-phenylcarbamoyl]-3H-indolium; iodide
CAS No.:126473-59-4
Molecular Formula:C₇₆H₆₆N₇O*I
Molecular Weight:1220.31
Hs Code.:

1-Ethyl-2-{(1E,3E,5E)-7-[1-ethyl-3,3-dimethyl-1,3-dihydro-indol-(2Z)-ylidene]-hepta-1,3,5-trienyl}-3,3-dimethyl-5-[4-((1Z,4Z,9Z,15Z)-10,15,20-triphenyl-porphyrin-5-yl)-phenylcarbamoyl]-3H-indolium; iodide

Synonyms:1-Ethyl-2-{(1E,3E,5E)-7-[1-ethyl-3,3-dimethyl-1,3-dihydro-indol-(2Z)-ylidene]-hepta-1,3,5-trienyl}-3,3-dimethyl-5-[4-((1Z,4Z,9Z,15Z)-10,15,20-triphenyl-porphyrin-5-yl)-phenylcarbamoyl]-3H-indolium; iodide

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Chemical Property of 1-Ethyl-2-{(1E,3E,5E)-7-[1-ethyl-3,3-dimethyl-1,3-dihydro-indol-(2Z)-ylidene]-hepta-1,3,5-trienyl}-3,3-dimethyl-5-[4-((1Z,4Z,9Z,15Z)-10,15,20-triphenyl-porphyrin-5-yl)-phenylcarbamoyl]-3H-indolium; iodide

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Technology Process of 1-Ethyl-2-{(1E,3E,5E)-7-[1-ethyl-3,3-dimethyl-1,3-dihydro-indol-(2Z)-ylidene]-hepta-1,3,5-trienyl}-3,3-dimethyl-5-[4-((1Z,4Z,9Z,15Z)-10,15,20-triphenyl-porphyrin-5-yl)-phenylcarbamoyl]-3H-indolium; iodide

There total 3 articles about 1-Ethyl-2-{(1E,3E,5E)-7-[1-ethyl-3,3-dimethyl-1,3-dihydro-indol-(2Z)-ylidene]-hepta-1,3,5-trienyl}-3,3-dimethyl-5-[4-((1Z,4Z,9Z,15Z)-10,15,20-triphenyl-porphyrin-5-yl)-phenylcarbamoyl]-3H-indolium; iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-97-7,30604-81-0
pyrrole

: 100-52-7
benzaldehyde

: 126442-94-2
1-Ethyl-2-{(1E,3E,5E)-7-[1-ethyl-3,3-dimethyl-1,3-dihydro-indol-(2Z)-ylidene]-hepta-1,3,5-trienyl}-5-(4-formyl-phenylcarbamoyl)-3,3-dimethyl-3H-indolium; iodide

: 917-23-7,20998-75-8
5,15,10,20-tetraphenylporphyrin

: 126473-59-4
1-Ethyl-2-{(1E,3E,5E)-7-[1-ethyl-3,3-dimethyl-1,3-dihydro-indol-(2Z)-ylidene]-hepta-1,3,5-trienyl}-3,3-dimethyl-5-[4-((1Z,4Z,9Z,15Z)-10,15,20-triphenyl-porphyrin-5-yl)-phenylcarbamoyl]-3H-indolium; iodide

Guidance literature:: With chloranil; trifluoroacetic acid; Yield given. Multistep reaction; 1.) CH₂Cl₂, room temperature, 1 h, 2.) CH₂Cl₂, ethanol, room temperature, 1 h;
DOI:10.1016/S0040-4020(01)85156-5

Reference yield:

: 126442-89-5
5-(4-acetamidophenyl)-10,15,20-tris(phenyl)porphyrin

: 126473-59-4
1-Ethyl-2-{(1E,3E,5E)-7-[1-ethyl-3,3-dimethyl-1,3-dihydro-indol-(2Z)-ylidene]-hepta-1,3,5-trienyl}-3,3-dimethyl-5-[4-((1Z,4Z,9Z,15Z)-10,15,20-triphenyl-porphyrin-5-yl)-phenylcarbamoyl]-3H-indolium; iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / trifluoroacetic acid, cc. aq. HCl / 21 h / 80 °C

2: 1.) triethylamine, 2.) N-phenylphosphoramidochloridate / 1.) CH₂Cl₂, room temperature, 5 min, 2.) CH₂Cl₂, 16 h

With hydrogenchloride; N-phenylphosphoramidochloridate; triethylamine; trifluoroacetic acid;
DOI:10.1016/S0040-4020(01)85156-5

Reference yield:

: 126442-88-4
1,1'-diethyl-3,3,3',3'-tetramethyl-5-carboxyindotricarbocyanine iodide

: 67605-64-5
5-(p-aminophenyl)-10,15,20-triphenylporphine

: 126473-59-4
1-Ethyl-2-{(1E,3E,5E)-7-[1-ethyl-3,3-dimethyl-1,3-dihydro-indol-(2Z)-ylidene]-hepta-1,3,5-trienyl}-3,3-dimethyl-5-[4-((1Z,4Z,9Z,15Z)-10,15,20-triphenyl-porphyrin-5-yl)-phenylcarbamoyl]-3H-indolium; iodide

Guidance literature:: With N-phenylphosphoramidochloridate; triethylamine; Yield given. Multistep reaction; 1.) CH₂Cl₂, room temperature, 5 min, 2.) CH₂Cl₂, 16 h;
DOI:10.1016/S0040-4020(01)85156-5