4-Cyano-4-(4-methoxy-phenyl)-2-oxo-cyclopentanecarboxylic acid tert-butyl ester

Base Information

Chemical Name:4-Cyano-4-(4-methoxy-phenyl)-2-oxo-cyclopentanecarboxylic acid tert-butyl ester
CAS No.:84409-24-5
Molecular Formula:C₁₈H₂₁NO₄
Molecular Weight:315.369
Hs Code.:

Synonyms:4-Cyano-4-(4-methoxy-phenyl)-2-oxo-cyclopentanecarboxylic acid tert-butyl ester

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Chemical Property of 4-Cyano-4-(4-methoxy-phenyl)-2-oxo-cyclopentanecarboxylic acid tert-butyl ester

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Technology Process of 4-Cyano-4-(4-methoxy-phenyl)-2-oxo-cyclopentanecarboxylic acid tert-butyl ester

There total 4 articles about 4-Cyano-4-(4-methoxy-phenyl)-2-oxo-cyclopentanecarboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 84409-18-7
3-Cyano-3-(4-methoxy-phenyl)-hexanedioic acid di-tert-butyl ester

: 84409-24-5
4-Cyano-4-(4-methoxy-phenyl)-2-oxo-cyclopentanecarboxylic acid tert-butyl ester

Guidance literature:: With sodium; In benzene; for 2.5h; Heating; other reagent (sodium amide);

Reference yield:

: 55710-80-0
tert-butyl 3-chloropropanoate

: 84409-24-5
4-Cyano-4-(4-methoxy-phenyl)-2-oxo-cyclopentanecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / aq.sodium hydroxide (40 percent), triethylbenzylammonium chloride / 2 h / 40 - 45 °C

2: 83 percent / sodium (powdered) / benzene / 2.5 h / Heating; other reagent (sodium amide)

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; sodium; In benzene;

Reference yield:

: 84409-14-3
(+/-)-tert-butyl 3-cyano-3-(4-methoxyphenyl)propanoate

: 84409-24-5
4-Cyano-4-(4-methoxy-phenyl)-2-oxo-cyclopentanecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / aq.sodium hydroxide (40 percent), triethylbenzylammonium chloride / 2 h / 40 - 45 °C

2: 83 percent / sodium (powdered) / benzene / 2.5 h / Heating; other reagent (sodium amide)

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; sodium; In benzene;