T-BUTYL 3-CHLOROPROPANOATE

Base Information

• Chemical Name: T-BUTYL 3-CHLOROPROPANOATE
• CAS No.: 55710-80-0
• Molecular Formula: C7H13ClO2
• Molecular Weight: 164.63000
• Hs Code.: 2915900090
• Mol file: 55710-80-0.mol

Synonyms:t-butyl chloropropionate;tert-butyl 3-chloropropionate;t-Butyl 3-chloropropanoate;Propanoic acid,3-chloro,1,1-dimethylethyl ester;

Chemical Property of T-BUTYL 3-CHLOROPROPANOATE

Chemical Property:

• Vapor Pressure: 0.769mmHg at 25°C
• Boiling Point: 183.5oC at 760 mmHg
• Flash Point: 68.5oC
• PSA: 26.30000
• Density: 1.035g/cm3
• LogP: 1.95700

Purity/Quality:

97% ^*data from raw suppliers

tert-butyl3-chloropropanoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of T-BUTYL 3-CHLOROPROPANOATE

There total 1 articles about T-BUTYL 3-CHLOROPROPANOATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloropropionic acid (107-94-8) + isobutene (115-11-7,15220-85-6) → tert-butyl 3-chloropropanoate (55710-80-0)

Guidance literature:

With sulfuric acid; tert-butyl alcohol; at -20 ℃;

Reference yield: 98.0%

tert-butyl 3-chloropropanoate (55710-80-0) + tert-butyl 3-cyano-3-phenylpropanoate (22485-02-5) → 3-Cyano-3-phenyl-hexanedioic acid di-tert-butyl ester (84409-16-5)

Guidance literature:

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; at 40 - 45 ℃; for 2h;

Reference yield: 95.0%

tert-butyl 3-chloropropanoate (55710-80-0) + (+/-)-tert-butyl 3-cyano-3-(2-methoxyphenyl)propanoate (84409-12-1) → 3-Cyano-3-(2-methoxy-phenyl)-hexanedioic acid di-tert-butyl ester (84409-20-1)

Guidance literature:

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; at 40 - 45 ℃; for 2h;

upstream raw materials:

chloropropionic acid

isobutene

Downstream raw materials:

3-Cyano-3-phenyl-hexanedioic acid di-tert-butyl ester

3-Cyano-3-(4-methoxy-phenyl)-hexanedioic acid di-tert-butyl ester

3-Cyano-3-(4-ethoxy-phenyl)-hexanedioic acid di-tert-butyl ester

3-Cyano-3-(2-methoxy-phenyl)-hexanedioic acid di-tert-butyl ester

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