C₃₃H₅₆O₈S₂Si

Base Information

Chemical Name:C₃₃H₅₆O₈S₂Si
CAS No.:1392829-10-5
Molecular Formula:C₃₃H₅₆O₈S₂Si
Molecular Weight:673.02
Hs Code.:

C<sub>33</sub>H<sub>56</sub>O<sub>8</sub>S<sub>2</sub>Si

Synonyms:C₃₃H₅₆O₈S₂Si

Suppliers and Price of C₃₃H₅₆O₈S₂Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₃H₅₆O₈S₂Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₃H₅₆O₈S₂Si

There total 15 articles about C₃₃H₅₆O₈S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1392829-00-3
C₁₆H₂₄O₂S₂

: 1392829-01-4
C₁₇H₃₂O₆Si

: 1392829-10-5
C₃₃H₅₆O₈S₂Si

Guidance literature:: C₁₆H₂₄O₂S₂; With n-butyllithium; In tetrahydrofuran; hexane; at -20 - 20 ℃; for 0.166667h; Inert atmosphere;

C₁₇H₃₂O₆Si; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.201503880

Reference yield:

: C₂₀H₃₀O₅Si

: 1392829-10-5
C₃₃H₅₆O₈S₂Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: boron trifluoride diethyl etherate / diethyl ether / 0 °C

2.1: sodium periodate; ruthenium trichloride; water; zinc(II) chloride / ethyl acetate; acetonitrile / 0 °C

3.1: toluene-4-sulfonic acid / tetrahydrofuran / 40 °C

4.1: sodium tetrahydroborate / methanol; dichloromethane / 0 °C

5.1: sodium hydride / tetrahydrofuran / 0 °C

5.2: 0 - 20 °C

6.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 80 °C

7.1: LiDBB / tetrahydrofuran / -78 °C

8.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 20 °C

9.1: n-butyllithium / tetrahydrofuran / 20 °C

9.2: -78 - 0 °C

With ruthenium trichloride; sodium tetrahydroborate; sodium periodate; n-butyllithium; 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; water; tri-n-butyl-tin hydride; sulfur trioxide pyridine complex; sodium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; zinc(II) chloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; ethyl acetate; acetonitrile; benzene; 6.1: Barton-McCombie deoxygenation / 8.1: Parikh-Doering oxidation;
DOI:10.1016/j.tetlet.2012.06.005

Reference yield:

: 1392829-16-1
C₂₄H₃₈O₇Si

: 1392829-10-5
C₃₃H₅₆O₈S₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium tetrahydroborate / methanol; dichloromethane / 0 °C

2.1: sodium hydride / tetrahydrofuran / 0 °C

2.2: 0 - 20 °C

3.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 80 °C

4.1: LiDBB / tetrahydrofuran / -78 °C

5.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 20 °C

6.1: n-butyllithium / tetrahydrofuran / 20 °C

6.2: -78 - 0 °C

With sodium tetrahydroborate; n-butyllithium; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sulfur trioxide pyridine complex; sodium hydride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; benzene; 3.1: Barton-McCombie deoxygenation / 5.1: Parikh-Doering oxidation;
DOI:10.1016/j.tetlet.2012.06.005