1-(2'-O-acetyl-5',6'-di-O-benzoyl-3'-O-mesyl-β-D-allofuranosyl)thymine

Base Information

Chemical Name:1-(2'-O-acetyl-5',6'-di-O-benzoyl-3'-O-mesyl-β-D-allofuranosyl)thymine
CAS No.:141980-95-2
Molecular Formula:C₂₈H₂₈N₂O₁₂S
Molecular Weight:616.603
Hs Code.:

Synonyms:1-(2'-O-acetyl-5',6'-di-O-benzoyl-3'-O-mesyl-β-D-allofuranosyl)thymine

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Chemical Property of 1-(2'-O-acetyl-5',6'-di-O-benzoyl-3'-O-mesyl-β-D-allofuranosyl)thymine

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Technology Process of 1-(2'-O-acetyl-5',6'-di-O-benzoyl-3'-O-mesyl-β-D-allofuranosyl)thymine

There total 4 articles about 1-(2'-O-acetyl-5',6'-di-O-benzoyl-3'-O-mesyl-β-D-allofuranosyl)thymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.5%

: C₂₅H₂₆O₁₂S

: 65-71-4,28806-14-6,691841-57-3
thymin

: 141980-95-2
1-(2'-O-acetyl-5',6'-di-O-benzoyl-3'-O-mesyl-β-D-allofuranosyl)thymine

Guidance literature:: With chloro-trimethyl-silane; trifluorormethanesulfonic acid; 1,1,1,3,3,3-hexamethyl-disilazane; In acetonitrile; for 12h; Heating;
DOI:10.1021/jm00094a014

Reference yield:

: 64993-88-0
1,2-O-isopropylidene-3-O-methanesulfonyl-α-D-allofuranose

: 141980-95-2
1-(2'-O-acetyl-5',6'-di-O-benzoyl-3'-O-mesyl-β-D-allofuranosyl)thymine

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent

2: AcOH, conc. H₂SO₄ / CH₂Cl₂ / 16 h / 4 °C

3: 68.5 percent / hexamethyldisilazane, chlorotrimethylsilane, trifluoromethanesulfonic acid / acetonitrile / 12 h / Heating

With chloro-trimethyl-silane; trifluorormethanesulfonic acid; sulfuric acid; acetic acid; 1,1,1,3,3,3-hexamethyl-disilazane; In dichloromethane; acetonitrile;
DOI:10.1021/jm00094a014

Reference yield:

: 98-88-4
benzoyl chloride

: 141980-95-2
1-(2'-O-acetyl-5',6'-di-O-benzoyl-3'-O-mesyl-β-D-allofuranosyl)thymine

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent

2: AcOH, conc. H₂SO₄ / CH₂Cl₂ / 16 h / 4 °C

3: 68.5 percent / hexamethyldisilazane, chlorotrimethylsilane, trifluoromethanesulfonic acid / acetonitrile / 12 h / Heating

With chloro-trimethyl-silane; trifluorormethanesulfonic acid; sulfuric acid; acetic acid; 1,1,1,3,3,3-hexamethyl-disilazane; In dichloromethane; acetonitrile;
DOI:10.1021/jm00094a014