9-[(3S,4S,5R)-4-Benzyloxy-5-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-thiophen-3-yl]-6-chloro-9H-purine

Base Information

• Chemical Name: 9-[(3S,4S,5R)-4-Benzyloxy-5-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-thiophen-3-yl]-6-chloro-9H-purine
• CAS No.: 206762-99-4
• Molecular Formula: C₃₃H₃₅ClN₄O₂SSi
• Molecular Weight: 615.271

Synonyms:9-[(3S,4S,5R)-4-Benzyloxy-5-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-thiophen-3-yl]-6-chloro-9H-purine

Chemical Property of 9-[(3S,4S,5R)-4-Benzyloxy-5-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-thiophen-3-yl]-6-chloro-9H-purine

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Technology Process of 9-[(3S,4S,5R)-4-Benzyloxy-5-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-thiophen-3-yl]-6-chloro-9H-purine

There total 1 articles about 9-[(3S,4S,5R)-4-Benzyloxy-5-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-thiophen-3-yl]-6-chloro-9H-purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

6-chloropurine (87-42-3) + (3S,4S,5R)-4-Benzyloxy-5-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-thiophen-3-ol (174833-54-6) → 9-[(3S,4S,5R)-4-Benzyloxy-5-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-thiophen-3-yl]-6-chloro-9H-purine (206762-99-4) + 9-[(3R,4S,5R)-4-Benzyloxy-5-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-thiophen-3-yl]-6-chloro-9H-purine

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; for 21h; Ambient temperature;

DOI:10.1021/jo980667s

Reference yield: 87.0%

9-[(3S,4S,5R)-4-Benzyloxy-5-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-thiophen-3-yl]-6-chloro-9H-purine (206762-99-4) → (2R,3S,4S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(6-chloro-purin-9-yl)-tetrahydro-thiophen-3-ol (214280-00-9)

Guidance literature:

With boron trichloride; In dichloromethane; for 0.5h; Ambient temperature;

DOI:10.1021/jo980667s

upstream raw materials:

6-chloropurine

(3S,4S,5R)-4-Benzyloxy-5-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-thiophen-3-ol

Downstream raw materials:

(2R,3S,4S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(6-chloro-purin-9-yl)-tetrahydro-thiophen-3-ol

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