C₃₃H₃₄N₂O₇

Base Information

Chemical Name:C₃₃H₃₄N₂O₇
CAS No.:1363373-59-4
Molecular Formula:C₃₃H₃₄N₂O₇
Molecular Weight:570.642
Hs Code.:

C<sub>33</sub>H<sub>34</sub>N<sub>2</sub>O<sub>7</sub>

Synonyms:C₃₃H₃₄N₂O₇

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Chemical Property of C₃₃H₃₄N₂O₇

Chemical Property:

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Technology Process of C₃₃H₃₄N₂O₇

There total 17 articles about C₃₃H₃₄N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99314-44-0
(3-methyloxetan-3-yl)methyl 4-methylbenzenesulfonate

: 1363373-59-4
C₃₃H₃₄N₂O₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: triethylamine; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 36 h / 70 °C / Inert atmosphere

2.1: boron trifluoride diethyl etherate / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

2.2: 0.5 h

3.1: dichloromethane / -78 °C / Inert atmosphere

3.2: 2.08 h / -78 °C / Inert atmosphere

3.3: 0.67 h / -78 - 0 °C

4.1: dichloromethane

5.1: oxalyl dichloride; dimethyl sulfoxide

6.1: -78 °C

7.1: water; acetic acid / tetrahydrofuran

8.1: hydrogen / palladium on activated charcoal

9.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide

With oxalyl dichloride; boron trifluoride diethyl etherate; water; hydrogen; tetra-(n-butyl)ammonium iodide; benzotriazol-1-ol; acetic acid; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 75867-41-3
4-trimethylsilanylethynyl-benzoic acid methyl ester

: 1363373-59-4
C₃₃H₃₄N₂O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; methanol / 3 h / 20 °C / Inert atmosphere

2.1: pyridine / copper diacetate / methanol / 24 h / 20 °C / Inert atmosphere

3.1: sodium hydroxide; methanol / 1 h / 20 °C / Reflux

3.2: pH 2

4.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide

With pyridine; methanol; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; copper diacetate; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 873-75-6
4-bromobenzenemethanol

: 1363373-59-4
C₃₃H₃₄N₂O₇

Guidance literature:: Multi-step reaction with 8 steps

1: 1H-imidazole / N,N-dimethyl-formamide

2: magnesium / tetrahydrofuran

3: dichloromethane

4: oxalyl dichloride; dimethyl sulfoxide

5: -78 °C

6: water; acetic acid / tetrahydrofuran

7: hydrogen / palladium on activated charcoal

8: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide

With 1H-imidazole; oxalyl dichloride; water; hydrogen; benzotriazol-1-ol; magnesium; acetic acid; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;